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Journal of Liquid Chromatography & Related Technologies Volume 30, 2007 - Issue 4
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Original Articles

Microextraction in Packed Syringe/Liquid Chromatography/Electrospray Tandem Mass Spectrometry for Quantification of Acebutolol and Metoprolol in Human Plasma and Urine Samples

Aziza El‐Beqqali University College of South Stockholm, Stockholm, Sweden
,
Anders Kussak University College of South Stockholm, Stockholm, Sweden
,
Lars Blomberg Karlstad University, Department of Chemistry, Karlstad, Sweden
&
Professor Mohamed Abdel‐Rehim AstraZeneca R&D Södertälje, Department of DMPK&BAC, Södertälje, SwedenCorrespondence[email protected]
Pages 575-586 | Received 05 Oct 2006, Accepted 03 Nov 2006, Published online: 07 Feb 2007

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Fernanda Helena Salami & Maria EugêniaC. Queiroz. (2014) MICROEXTRACTION IN PACKED SORBENT FOR ANALYSIS OF SULFONAMIDES IN POULTRY LITTER WASTEWATER SAMPLES BY LIQUID CHROMATOGRAPHY AND SPECTROPHOTOMETRIC DETECTION. Journal of Liquid Chromatography & Related Technologies 37:16, pages 2377-2388.
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Cláudia Ribeiro, Ana Rita Ribeiro, Alexandra S. Maia, Virgínia M. F. Gonçalves & Maria Elizabeth Tiritan. (2014) New Trends in Sample Preparation Techniques for Environmental Analysis. Critical Reviews in Analytical Chemistry 44:2, pages 142-185.
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Rana Said, Zuzan Hassan, Moustapha Hassan & Mohamed Abdel‐Rehim. (2008) Rapid and Sensitive Method for Determination of Cyclophosphamide in Patients Plasma Samples Utilizing Microextraction by Packed Sorbent Online with Liquid Chromatography‐Tandem Mass Spectrometry (MEPS‐LC‐MS/MS). Journal of Liquid Chromatography & Related Technologies 31:5, pages 683-694.
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Articles from other publishers (49)

Angela Arcoleo, Federica Bianchi & Maria Careri. (2021) A sensitive microextraction by packed sorbent-gas chromatography-mass spectrometry method for the assessment of polycyclic aromatic hydrocarbons contamination in Antarctic surface snow. Chemosphere 282, pages 131082.
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Mohamed Abdel-Rehim, Stig Pedersen-Bjergaard, Abbi Abdel-Rehim, Rafael Lucena, Mohammad Mahdi Moein, Soledad Cárdenas & Manuel Miró. (2020) Microextraction approaches for bioanalytical applications: An overview. Journal of Chromatography A 1616, pages 460790.
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Cheng Yan, Guihua Duan, Yi Pan, Fang-Xiang Wu & Jianxin Wang. (2019) DDIGIP: predicting drug-drug interactions based on Gaussian interaction profile kernels. BMC Bioinformatics 20:S15.
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Hanieh Karimiyan, Mohammad Reza Hadjmohammadi, Karthik Laxman Kunjali, Mohammad Mahdi Moein, Joydeep Dutta & Mohamed Abdel-Rehim. (2019) Graphene Oxide/Polyethylene Glycol-Stick for Thin Film Microextraction of β-Blockers from Human Oral Fluid by Liquid Chromatography-Tandem Mass Spectrometry. Molecules 24:20, pages 3664.
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Gaurav Dhingra, Pooja Bansal, Nidhi Dhingra, Susheela Rani & Ashok Kumar Malik. (2018) Development of a microextraction by packed sorbent with gas chromatography-mass spectrometry method for quantification of nitroexplosives in aqueous and fluidic biological samples. Journal of Separation Science 41:3, pages 639-647.
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Liu Yang, Rana Said & Mohamed Abdel-Rehim. (2017) Sorbent, device, matrix and application in microextraction by packed sorbent (MEPS): A review. Journal of Chromatography B 1043, pages 33-43.
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Mohammad Mahdi Moein, Aziza El Beqqali & Mohamed Abdel-Rehim. (2017) Bioanalytical method development and validation: Critical concepts and strategies. Journal of Chromatography B 1043, pages 3-11.
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Tamara Ballesteros-Esteban, Emilia M Reyes-Gallardo, Rafael Lucena, Soledad Cárdenas & Miguel Valcárcel. (2016) Determination of propranolol and carvedilol in urine samples using a magnetic polyamide composite and LC–MS/MS. Bioanalysis 8:20, pages 2115-2123.
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Hatem Elmongy, Hytham Ahmed, Abdel-Aziz Wahbi, Ahmad Amini, Anders Colmsjö & Mohamed Abdel-Rehim. (2016) Determination of metoprolol enantiomers in human plasma and saliva samples utilizing microextraction by packed sorbent and liquid chromatography-tandem mass spectrometry. Biomedical Chromatography 30:8, pages 1309-1317.
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Mohammad Mahdi Moein, Abbi Abdel-Rehim & Mohamed Abdel-Rehim. (2015) Microextraction by packed sorbent (MEPS). TrAC Trends in Analytical Chemistry 67, pages 34-44.
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Malgorzata Szultka, Pawel Pomastowski, Viorica Railean-Plugaru & Boguslaw Buszewski. (2014) Microextraction sample preparation techniques in biomedical analysis. Journal of Separation Science 37:21, pages 3094-3105.
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Jorge Pereira, José S. Câmara, Anders Colmsjö & Mohamed Abdel-Rehim. (2014) Microextraction by packed sorbent: an emerging, selective and high-throughput extraction technique in bioanalysis. Biomedical Chromatography 28:6, pages 839-847.
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Agneša Páleníková & Svetlana Hrouzková. (2014) Microextraction in packed syringe: solvent-minimized sample preparation technique. Monatshefte für Chemie - Chemical Monthly 145:4, pages 537-549.
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Wei Du, Chunmei Lei, Siruo Zhang, Gang Bai, Huiyan Zhou, Min Sun, Qiang Fu & Chun Chang. (2014) Determination of clenbuterol from pork samples using surface molecularly imprinted polymers as the selective sorbents for microextraction in packed syringe. Journal of Pharmaceutical and Biomedical Analysis 91, pages 160-168.
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Jialiang Pan, Chengjiang Zhang, Zhuomin Zhang & Gongke Li. (2014) Review of online coupling of sample preparation techniques with liquid chromatography. Analytica Chimica Acta 815, pages 1-15.
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Jorge Pereira, Catarina Luís Silva, Rosa Perestrelo, João Gonçalves, Vera Alves & José S. Câmara. (2014) Re-exploring the high-throughput potential of microextraction techniques, SPME and MEPS, as powerful strategies for medical diagnostic purposes. Innovative approaches, recent applications and future trends. Analytical and Bioanalytical Chemistry 406:8, pages 2101-2122.
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Catarina Silva, Carina Cavaco, Rosa Perestrelo, Jorge Pereira & José Câmara. (2014) Microextraction by Packed Sorbent (MEPS) and Solid-Phase Microextraction (SPME) as Sample Preparation Procedures for the Metabolomic Profiling of Urine. Metabolites 4:1, pages 71-97.
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Mohammad Mahdi Moein, Rana Said, Fatma Bassyouni & Mohamed Abdel-Rehim. (2014) Solid Phase Microextraction and Related Techniques for Drugs in Biological Samples. Journal of Analytical Methods in Chemistry 2014, pages 1-24.
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Fernanda H. Salami & Maria Eugênia C. Queiroz. (2013) Microextraction in Packed Sorbent for the Determination of Pesticides in Honey Samples by Gas Chromatography Coupled to Mass Spectrometry. Journal of Chromatographic Science 51:10, pages 899-904.
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Seyed Mosayeb Daryanavard, Amin Jeppsson-Dadoun, Lars I. Andersson, Mahdi Hashemi, Anders Colmsjö & Mohamed Abdel-Rehim. (2013) Molecularly imprinted polymer in microextraction by packed sorbent for the simultaneous determination of local anesthetics: lidocaine, ropivacaine, mepivacaine and bupivacaine in plasma and urine samples. Biomedical Chromatography 27:11, pages 1481-1488.
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Abbi Abdel-Rehim & Mohamed Abdel-Rehim. (2013) Evaluation of microextraction by packed sorbent and micro-liquid chromatography-tandem mass spectrometry as a green approach in bioanalysis. Biomedical Chromatography 27:10, pages 1225-1233.
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Abbi Abdel‐Rehim & Mohamed Abdel‐Rehim. (2013) Screening and determination of drugs in human saliva utilizing microextraction by packed sorbent and liquid chromatography–tandem mass spectrometry. Biomedical Chromatography 27:9, pages 1188-1191.
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Gilberto AlvesMárcio Rodrigues, Ana Fortuna, Amílcar Falcão & João Queiroz. (2013) A critical review of microextraction by packed sorbent as a sample preparation approach in drug bioanalysis. Bioanalysis 5:11, pages 1409-1442.
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Christina Skoglund, Fatma Bassyouni & Mohamed Abdel‐Rehim. (2012) Monolithic packed 96‐tips set for high‐throughput sample preparation: determination of cyclophosphamide and busulfan in whole blood samples by monolithic packed 96‐tips and LC‐MS. Biomedical Chromatography 27:6, pages 714-719.
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Irena Baranowska, Sylwia Magiera & Jacek Baranowski. (2013) Clinical applications of fast liquid chromatography: A review on the analysis of cardiovascular drugs and their metabolites. Journal of Chromatography B 927, pages 54-79.
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Nadia Y. Ashri, Mosayeb Daryanavard & Mohamed Abdel‐Rehim. (2012) Microextraction by packed sorbent and liquid chromatography–tandem mass spectrometry as a tool for quantification of peptides in plasma samples: determination of sensory neuron‐specific receptors agonist BAM8‐22 and antagonist BAM22‐8 in plasma samples. Biomedical Chromatography 27:3, pages 396-403.
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Márcio Rodrigues, Gilberto Alves, Marília Rocha, João Queiroz & Amílcar Falcão. (2013) First liquid chromatographic method for the simultaneous determination of amiodarone and desethylamiodarone in human plasma using microextraction by packed sorbent (MEPS) as sample preparation procedure. Journal of Chromatography B 913-914, pages 90-97.
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Katrine Nielsen, Frants R. Lauritsen, Teemu Nissilä & Raimo A. Ketola. (2011) Rapid screening of drug compounds in urine using a combination of microextraction by packed sorbent and rotating micropillar array electrospray ionization mass spectrometry. Rapid Communications in Mass Spectrometry 26:3, pages 297-303.
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Hana Vlčková, Martina Rabatinová, Alena Mikšová, Gabriela Kolouchová, Stanislav Mičuda, Petr Solich & Lucie Nováková. (2012) Determination of pravastatin and pravastatin lactone in rat plasma and urine using UHPLC–MS/MS and microextraction by packed sorbent. Talanta 90, pages 22-29.
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Berta Mendes, João Gonçalves & José S. Câmara. (2012) Effectiveness of high-throughput miniaturized sorbent- and solid phase microextraction techniques combined with gas chromatography–mass spectrometry analysis for a rapid screening of volatile and semi-volatile composition of wines—A comparative study. Talanta 88, pages 79-94.
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N. Etxebarria, P. Navarro, A. Prieto, M. Olivares, A. Usobiaga, L. A. Fernández & Olatz Zuloaga. 2012. Environmental Chemistry for a Sustainable World. Environmental Chemistry for a Sustainable World 171 235 .
A. Prieto, A. Vallejo, O. Zuloaga, A. Paschke, B. Sellergen, E. Schillinger, S. Schrader & M. Möder. (2011) Selective determination of estrogenic compounds in water by microextraction by packed sorbents and a molecularly imprinted polymer coupled with large volume injection-in-port-derivatization gas chromatography–mass spectrometry. Analytica Chimica Acta 703:1, pages 41-51.
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Nadia Y Ashri & Mohamed Abdel-Rehim. (2011) Sample treatment based on extraction techniques in biological matrices. Bioanalysis 3:17, pages 2003-2018.
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Mohamed Abdel-Rehim. (2011) Microextraction by packed sorbent (MEPS): A tutorial. Analytica Chimica Acta 701:2, pages 119-128.
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Susheela Rani, Ashwini Kumar, Ashok Kumar Malik & Baldev Singh. (2011) Quantification of Tricyclic and Nontricyclic Antidepressants in Spiked Plasma and Urine Samples Using Microextraction in Packed Syringe and Analysis by LC and GC-MS. Chromatographia 74:3-4, pages 235-242.
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Sandra Pérez, Marinella Farré, Carlos Gonçalves, Jaume Aceña, M. F. Alpendurada & Damià Barceló. 2011. Challenges in Green Analytical Chemistry. Challenges in Green Analytical Chemistry 224 285 .
Hana Vlčková, Dagmar Solichová, Milan Bláha, Petr Solich & Lucie Nováková. (2011) Microextraction by packed sorbent as sample preparation step for atorvastatin and its metabolites in biological samples—Critical evaluation. Journal of Pharmaceutical and Biomedical Analysis 55:2, pages 301-308.
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Andréa R. Chaves, Fernanda Z. Leandro, Juciene A. Carris & Maria Eugênia C. Queiroz. (2010) Microextraction in packed sorbent for analysis of antidepressants in human plasma by liquid chromatography and spectrophotometric detection. Journal of Chromatography B 878:23, pages 2123-2129.
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Monika Moeder, Steffi Schrader, Ursula Winkler & Rosario Rodil. (2010) At-line microextraction by packed sorbent-gas chromatography–mass spectrometry for the determination of UV filter and polycyclic musk compounds in water samples. Journal of Chromatography A 1217:17, pages 2925-2932.
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Mohamed Abdel-Rehim. (2010) Recent advances in microextraction by packed sorbent for bioanalysis. Journal of Chromatography A 1217:16, pages 2569-2580.
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Rana Said, Mohamed Kamel, Aziza El-Beqqali & Mohamed Abdel-Rehim. (2010) Microextraction by packed sorbent for LC–MS/MS determination of drugs in whole blood samples. Bioanalysis 2:2, pages 197-205.
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Hiroyuki Kataoka. (2009) Recent developments and applications of microextraction techniques in drug analysis. Analytical and Bioanalytical Chemistry 396:1, pages 339-364.
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Lucie Nováková & Hana Vlčková. (2009) A review of current trends and advances in modern bio-analytical methods: Chromatography and sample preparation. Analytica Chimica Acta 656:1-2, pages 8-35.
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Mohamed Abdel-Rehim. (2009) Microextraction by packed sorbent in bioanalysis. Bioanalysis 1:4, pages 687-691.
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Eshwar Jagerdeo & Mohamed Abdel-Rehim. (2011) Screening of cocaine and its metabolites in human urine samples by direct analysis in real-time source coupled to time-of-flight mass spectrometry after online preconcentration utilizing microextraction by packed sorbent. Journal of the American Society for Mass Spectrometry 20:5, pages 891-899.
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Gabriel Morales-Cid, Soledad Cárdenas, Bartolomé M. Simonet & Miguel Valcárcel. (2009) Direct automatic determination of free and total anesthetic drugs in human plasma by use of a dual (microdialysis-microextraction by packed sorbent) sample treatment coupled at-line to NACE-MS. ELECTROPHORESIS 30:10, pages 1684-1691.
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Lars G. Blomberg. (2008) Two new techniques for sample preparation in bioanalysis: Microextraction in packed sorbent (MEPS) and use of a bonded monolith as sorbent for sample preparation in polypropylene tips for 96-well plates. Analytical and Bioanalytical Chemistry 393:3, pages 797-807.
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Zeki Altun & Mohamed Abdel-Rehim. (2008) Study of the factors affecting the performance of microextraction by packed sorbent (MEPS) using liquid scintillation counter and liquid chromatography-tandem mass spectrometry. Analytica Chimica Acta 630:2, pages 116-123.
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. (2007) Current literature in mass spectrometry. Journal of Mass Spectrometry 42:9, pages 1251-1262.
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