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Journal of Liquid Chromatography Volume 15, 1992 - Issue 1
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Original Articles

Determination of Enantiomers in Human Serum by Direct Injection onto a β-Cyclodextrin HPLC Bonded Phase

Apryll M. Stalcup Department of Chemistry 2545 The Mall, University of Hawaii at Manoa, Honolulu, Hawaii, 96822
&
Karen L. Williams Department of Chemistry 2545 The Mall, University of Hawaii at Manoa, Honolulu, Hawaii, 96822
Pages 29-37 | Published online: 23 Sep 2006

Citations (33)

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Read on this site (3)

Guy Felix & Alain Berthod. (2008) Part II: From Dermatologicals to Sensory Organ and Various Drugs. Separation & Purification Reviews 37:1-2, pages 1-227.
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Guy Felix & Alain Berthod. (2007) Commercial Chiral Stationary Phases for the Separations of Clinical Racemic Drugs. Separation & Purification Reviews 36:4, pages 285-481.
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CurtisN. Nakatsu & ApryllM. Stalcup. (1993) Separation of Enantiomers Using an (S)-Naphthylethylcarbamoylated γ-Cyclodextrin Stationary Phase. Journal of Liquid Chromatography 16:1, pages 209-223.
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Articles from other publishers (30)

Ana R. Ribeiro, Alexandra S. Maia, Quezia B. Cass & Maria E. Tiritan. (2014) Enantioseparation of chiral pharmaceuticals in biomedical and environmental analyses by liquid chromatography: An overview. Journal of Chromatography B 968, pages 8-21.
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Peter A. L. Jacobsen, Jeppe L. Nielsen, Maria V. Juhl, Naseem Theilgaard & Kim L. Larsen. (2011) Grafting cyclodextrins to calcium phosphate ceramics for biomedical applications. Journal of Inclusion Phenomena and Macrocyclic Chemistry 72:1-2, pages 173-181.
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Ronit Freeman & Itamar Willner. (2012) Optical molecular sensing with semiconductor quantum dots (QDs). Chemical Society Reviews 41:10, pages 4067.
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Ronnie Nielsen, Peter Kingshott, Tamer Uyar, Jale Hacaloglu & Kim L. Larsen. (2011) Characterization of β-cyclodextrin modified SiO 2 . Surface and Interface Analysis 43:5, pages 884-892.
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Frank Davis & Séamus Higson. 2011. Macrocycles. Macrocycles 190 254 .
Ronit Freeman, Jian-Ping Xu & Itamar Willner. 2010. Nanoparticles. Nanoparticles 455 511 .
Ronnie Nielsen, Jeppe L. Nielsen & Kim L. Larsen. (2009) Distribution and accessibility of cyclodextrins covalently bound onto silica gel. Journal of Inclusion Phenomena and Macrocyclic Chemistry 67:3-4, pages 399-405.
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Ronit Freeman, Tali Finder, LiLy Bahshi & Itamar Willner. (2009) β-Cyclodextrin-Modified CdSe/ZnS Quantum Dots for Sensing and Chiroselective Analysis. Nano Letters 9:5, pages 2073-2076.
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David S. Van Meter, Nyoté J. Oliver, A. Björn Carle, Sabine Dehm, Thomas H. Ridgway & Apryll M. Stalcup. (2008) Characterization of surface-confined ionic liquid stationary phases: impact of cation and anion identity on retention. Analytical and Bioanalytical Chemistry 393:1, pages 283-294.
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G. Félix & D. Campèse. (2007) Development of a New RAM-Chiral Column for Determination of Chiral Drugs in Biological Fluids by HPLC. Chromatographia 66:3-4, pages 159-164.
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Myung Ho Hyun, Yanci Song, Yoon Jae Cho & Do Hun Kim. (2006) Preparation of a new doubly tethered chiral stationary phase based on (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid and its application. Journal of Chromatography A 1108:2, pages 208-217.
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X. Han, Q. Zhong, D. Yue, N. Della C�, R. C. Larock & D. W. Armstrong. (2005) Separation of Enantiomers of Isochromene Derivatives by HPLC Using Cyclodextrin-Based Stationary Phases. Chromatographia 61:5-6, pages 205-211.
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Myung Ho Hyun, Do Hun Kim, Yoon Jae Cho & Jong Sung Jin. (2005) Preparation and evaluation of a doubly tethered chiral stationary phase based on (+)‐(18‐crown‐6)‐2,3,11,12‐tetracarboxylic acid. Journal of Separation Science 28:5, pages 421-427.
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Anne Ponchel, Sébastien Abramson, Juliette Quartararo, Denis Bormann, Yolande Barbaux & Eric Monflier. (2004) Cyclodextrin silica-based materials: advanced characterizations and study of their complexing behavior by diffuse reflectance UV–Vis spectroscopy. Microporous and Mesoporous Materials 75:3, pages 261-272.
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. (2004) Effect of the Protection of the Residual Aminopropyl Groups of a Chiral Stationary Phase Based on (+)-(18-Crown-6)-2,3,11,12-tetracarboxylic Acid on the Chiral Resolution Behaviors. Bulletin of the Korean Chemical Society 25:3, pages 400-402.
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Myung Ho Hyun & Do Hun Kim. (2004) Spacer length effect of a chiral stationary phase based on (+)‐(18‐crown‐6)‐2,3,11,12‐tetracarboxylic acid. Chirality 16:5, pages 294-301.
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Hassan Aboul-Enein & Imran Ali. 2003. Chiral Separations By Liquid Chromatography And Related Technologies. Chiral Separations By Liquid Chromatography And Related Technologies 89 136 .
Myung H Hyun, Yoon Jae Cho, Jin Ah Kim & Jong Sung Jin. (2003) Preparation and application of a new modified liquid chromatographic chiral stationary phase based on (+)-(18-crown-6)-2,3,11,12-tetracarboxylic acid. Journal of Chromatography A 984:2, pages 163-171.
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Gregorio Crini & Michel Morcellet. (2002) Synthesis and applications of adsorbents containing cyclodextrins. Journal of Separation Science 25:13, pages 789-813.
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Myung Ho Hyun, Sang Cheol Han, Cheong Wha Lee & Yun Kyeong Lee. (2002) Preparation and application of a new ligand exchange chiral stationary phase for the liquid chromatographic resolution of α-amino acid enantiomers. Journal of Chromatography A 950:1-2, pages 55-63.
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Jong Sung Jin, Apryll M. Stalcup & Myung Ho Hyun. (2001) Impact of triethylamine as a mobile phase additive on the resolution of racemic amino acids on an (+)-18-crown-6-tetracarboxylic acid-derived chiral stationary phase. Journal of Chromatography A 933:1-2, pages 83-90.
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Apryll M. Stalcup, Kyung H. Gahm, Samuel R. Gratz & Richard M. C. Sutton. (1998) Application of Classical Gel Electrophoresis to the Chiral Separation of Milligram Quantities of Terbutaline. Analytical Chemistry 70:1, pages 144-148.
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Claudio Giachetti, Anna Tenconi, Sergio Canali & Giovanni Zanolo. (1997) Simultaneous determination of atenolol and chlorthalidone in plasma by high-performance liquid chromatography application to pharmacokinetic studies in man. Journal of Chromatography B: Biomedical Sciences and Applications 698:1-2, pages 187-194.
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Apryll M. Stalcup, Wenhong Wu & Karen L. Williams. (1997) Separation of benzodiazepines on a new carbohydrate-based chiral stationary phase for HPLC. Biomedical Chromatography 11:5, pages 325-330.
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Soon M. Han. (1997) Direct enantiomeric separations by high performance liquid chromatography using cyclodextrins. Biomedical Chromatography 11:5, pages 259-271.
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Françoise Bressolle, Michel Audran, Tuyet-Nga Pham & Jean-Jacques Vallon. (1996) Cyclodextrins and enantiomeric separations of drugs by liquid chromatography and capillary electrophoresis: basic principles and new developments. Journal of Chromatography B: Biomedical Sciences and Applications 687:2, pages 303-336.
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C. Moeder, T. O'Brien, R. Thompson & G. Bicker. (1996) Determination of stoichiometric coefficients and apparent formation constants for α- and β-CD complexes of terpenes using reversed-phase liquid chromatography. Journal of Chromatography A 736:1-2, pages 1-9.
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Apryll M. Stalcup & Karen L. Williams. (1995) Comparison of 1-(1-naphthy)ethylcarbamate derivatives of a carbohydrate bonded chiral stationary phase. Journal of Chromatography A 695:2, pages 185-193.
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Karen L. Williams & Apryll M. Stalcup. 1993. Molecular Interactions in Bioseparations. Molecular Interactions in Bioseparations 189 202 .
Christian Roussel & Anita Favrou. (2004) γ‐Cyclodextrin as chiral mobile phase additive in the HPLC separation of the atropisomers of some N ‐arylthiazoline‐2‐thiones and N ‐arylthiazoline‐2‐ones: Attempts to quantify the effect of selected structural parameters . Chirality 5:6, pages 471-478.
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