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American Industrial Hygiene Association Journal Volume 57, 1996 - Issue 10
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Original Articles

Development of a Novel Derivatization Reagent for the Sampling and Analysis of Total Isocyanate Group in Air and Comparison of its Performance with that of Several Established Reagents

Robert P. Streicher Department of Health and Human Services, U.S. Public Health Service, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health, Division of Physical Sciences and Engineering, 4676 Columbia Parkway, Cincinnati, OH 45226
,
James E. Arnold Department of Health and Human Services, U.S. Public Health Service, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health, Division of Physical Sciences and Engineering, 4676 Columbia Parkway, Cincinnati, OH 45226
,
M. Kathleen Ernst Department of Health and Human Services, U.S. Public Health Service, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health, Division of Physical Sciences and Engineering, 4676 Columbia Parkway, Cincinnati, OH 45226
&
Charles V. Cooper Department of Health and Human Services, U.S. Public Health Service, Centers for Disease Control and Prevention, National Institute for Occupational Safety and Health, Division of Physical Sciences and Engineering, 4676 Columbia Parkway, Cincinnati, OH 45226
Pages 905-913 | Published online: 04 Jun 2010

Citations (28)

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Susana Garcia-Alonso & Rosa María Perez-Pastor. (2020) Organic Analysis of Environmental Samples Using Liquid Chromatography with Diode Array and Fluorescence Detectors: An Overview. Critical Reviews in Analytical Chemistry 50:1, pages 29-49.
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JoshuaW. Schaeffer, Layne Marie Sargent, DelvinR. Sandfort & WilliamJ. Brazile. (2013) A Comparison of Two Sampling Methods for the Detection of Airborne Methylene Bisphenyl Diisocyanate. Journal of Occupational and Environmental Hygiene 10:4, pages 213-221.
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W.E. Rudzinski, J. Yin, T. Anderson, S. Norman, G. Unnikrishnan, J.T. Varkey, S.C. George, S. Thomas & T.M. Aminabhavi. (1998) Preparation and Evaluation of Polyuretham Foam/Rubber Membrane-Based Samplers for use in Isocyanate Sampling. Polymer-Plastics Technology and Engineering 37:1, pages 103-113.
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J. Thomas Pierce. (1995) Conference Summary: The Value of Short Case Reports—56th Annual American Industrial Hygiene Conference and Exposition. Applied Occupational and Environmental Hygiene 10:10, pages 803-811.
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Articles from other publishers (24)

Glen McConnachie & Paul Johnson. (2023) Total Reactive Isocyanate Group (TRIG) Measurement: A Commentary. Annals of Work Exposures and Health 67:5, pages 553-558.
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S. Selvakumar, Subbaraj Karunakaran & V. Siva Rama Krishna. (2022) Detection techniques for air-borne isocyanates based on fluorescent derivatizing agents. Environmental Science: Atmospheres 2:6, pages 1249-1258.
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Linda Bengtström, Mariëlle Salden & Anna A. Stec. (2016) The role of isocyanates in fire toxicity. Fire Science Reviews 5:1.
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Homero Harari, Dhimiter Bello, Susan Woskie & Carrie Redlich. (2016) Development of an Interception Glove Sampler for Skin Exposures to Aromatic Isocyanates. Annals of Occupational Hygiene 60:9, pages 1092-1103.
Crossref
Rolf M.A. Hahne & Ryan F. LeBouf. 2007. Encyclopedia of Analytical Chemistry. Encyclopedia of Analytical Chemistry 1 33 .
Humberto E. Ferreira, José A. D. Condeço, Inês O. Fernandes, David E. Duarte & João C. M. Bordado. (2014) HPLC-UV and HPLC-ESI + -MS/MS analysis of free monomeric methylene diphenyl diisocyanate in polyurethane foams and prepolymers after stabilization with NBMA a new derivatizating agent . Anal. Methods 6:23, pages 9242-9257.
Crossref
Dick Heederik, Lygia Budnik, Brigitte Roberge & Nicole Goyer. 2013. Asthma in the Workplace. Asthma in the Workplace 85 98 .
Diana M. Ceballos, Stephen G. Whittaker, Michael G. Yost, Russell L. Dills, Dhimiter Bello, Jennifer M. Thomasen, Leena A. Nylander-French, Carolyn K. Reeb-Whitaker, Phillip M. Peters, Elisa C. Weiland & Wallace W. Suydam. (2011) A laboratory comparison of analytical methods used for isocyanates. Analytical Methods 3:11, pages 2478.
Crossref
. (2008) Validation of Transferability of DBA Derivatization and LC–MS/MS Determination Method for Isocyanates via an Interlaboratory Comparison. The Annals of Occupational Hygiene.
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. (2008) Size-Separated Sampling and Analysis of Isocyanates in Workplace Aerosols. Part I. Denuder—Cascade Impactor Sampler. The Annals of Occupational Hygiene.
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Samuel P. Tucker. (2007) Investigation of reagent distributions on glass fiber membrane filters used in air sampling. Journal of Environmental Monitoring 9:10, pages 1122.
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Hartmut Henneken, Martin Vogel & Uwe Karst. (2006) Determination of airborne isocyanates. Analytical and Bioanalytical Chemistry 387:1, pages 219-236.
Crossref
Jacques Lesage & Guy Perrault. 2006. Asthma in the Workplace, Third Edition. Asthma in the Workplace, Third Edition 297 318 .
Daniel Karlsson, Jakob Dahlin, Åsa Marand, Gunnar Skarping & Marianne Dalene. (2005) Determination of airborne isocyanates as di-n-butylamine derivatives using liquid chromatography and tandem mass spectrometry. Analytica Chimica Acta 534:2, pages 263-269.
Crossref
Bettina Seiwert, Hartmut Henneken & Uwe Karst. (2004) Ferrocenoyl piperazide as derivatizing agent for the analysis of isocyanates and related compounds using liquid chromatography/electrochemistry/mass spectrometry (LC/EC/MS). Journal of the American Society for Mass Spectrometry 15:12, pages 1727-1736.
Crossref
Sabine Werlich, Heidi Stockhorst, Ute Witting & Norbert Binding. (2004) MMNTP—a new tailor-made modular derivatization agent for the selective determination of isocyanates and diisocyanates. The Analyst 129:4, pages 364-370.
Crossref
Erik Vangronsveld & Friedrich Mandel. (2003) Workplace monitoring of isocyanates using ion trap liquid chromatography/tandem mass spectrometry. Rapid Communications in Mass Spectrometry 17:15, pages 1685-1690.
Crossref
Martin Vogel & Uwe Karst. (2002) 4-Nitro-7-piperazino-2,1,3-benzoxadiazole as a Reagent for Monitoring of Airborne Isocyanates by Liquid Chromatography. Analytical Chemistry 74:24, pages 6418-6426.
Crossref
Peter von Zweigbergk, Roger Lindahl, Anders Östin, Jenny Ekman & Jan-Olof Levin. (2002) Development of a diffusive sampling method for determination of methyl isocyanate in air. J. Environ. Monit. 4:5, pages 663-666.
Crossref
Rolf M.A. Hahne. 2007. Encyclopedia of Analytical Chemistry. Encyclopedia of Analytical Chemistry.
E. B. Guglya. (2000) Determination of isocyanates in air. Journal of Analytical Chemistry 55:6, pages 508-529.
Crossref
An-Soo Jang, Inseon-S. Choi, Young Il Koh, Jai-Dong Moon & Kang-Jin Lee. (2000) Increase in airway hyperresponsiveness among workers exposed to methylene diphenyldiisocyanate compared to workers exposed to toluene diisocyanate at a petrochemical plant in Korea. American Journal of Industrial Medicine 37:6, pages 663-667.
Crossref
William M. Draper, Kevin Ashley, Clifford R. Glowacki & Paul R. Michael. (1999) Industrial Hygiene Chemistry:  Keeping Pace with Rapid Change in the Workplace. Analytical Chemistry 71:12, pages 33-60.
Crossref
John G. Dorsey, William T. Cooper, Barbara A. Siles, Joe P. Foley & Howard G. Barth. (1998) Liquid Chromatography:  Theory and Methodology. Analytical Chemistry 70:12, pages 591-644.
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