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Food Additives & Contaminants: Part A Volume 28, 2011 - Issue 11
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Original Articles

Determination of tadalafil and N-desmethylsibutramine in health and dietary supplements using ultra-performance liquid chromatography (UPLC) coupled with quadrupole-time-of-flight mass spectrometry (Q-TOF MS)

S.H. Roh College of Pharmacy and Research Institute of Pharmaceutical Sciences, Seoul National University, Seoul 151-742, Republic of Korea
,
Y.P. Kang College of Pharmacy and Research Institute of Pharmaceutical Sciences, Seoul National University, Seoul 151-742, Republic of Korea
,
S. Park College of Pharmacy and Research Institute of Pharmaceutical Sciences, Seoul National University, Seoul 151-742, Republic of Korea
,
Y. Huh College of Pharmacy and Research Institute of Pharmaceutical Sciences, Seoul National University, Seoul 151-742, Republic of Korea
,
J. Lee College of Pharmacy, Sungkyunkwan University, Suwon 440-746, Republic of Korea
,
J.H. Park College of Pharmacy and Research Institute of Pharmaceutical Sciences, Seoul National University, Seoul 151-742, Republic of Korea
,
D. Kim College of Pharmacy and Research Institute of Pharmaceutical Sciences, Seoul National University, Seoul 151-742, Republic of Korea
&
S.W. Kwon College of Pharmacy and Research Institute of Pharmaceutical Sciences, Seoul National University, Seoul 151-742, Republic of KoreaCorrespondence[email protected]
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Pages 1475-1482 | Received 10 Mar 2011, Accepted 24 Jun 2011, Published online: 09 Aug 2011

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Samin Hamidi. (2023) Assessment of Undeclared Synthetic Drugs in Dietary Supplements in an Analytical View: A Comprehensive Review. Critical Reviews in Analytical Chemistry 53:5, pages 986-996.
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Articles from other publishers (21)

Nurşen Başaran, Duygu Paslı & A. Ahmet Başaran. (2022) Unpredictable adverse effects of herbal products. Food and Chemical Toxicology 159, pages 112762.
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Beom Hee Kim, Wonwoong Lee, You Lee Kim, Ji Hyun Lee & Jongki Hong. (2021) Efficient Matrix Cleanup of Soft-Gel-Type Dietary Supplements for Rapid Screening of 92 Illegal Adulterants Using EMR-Lipid dSPE and UHPLC-Q/TOF-MS. Pharmaceuticals 14:6, pages 570.
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Liliana Muschietti, Flavia Redko & Jerónimo Ulloa. (2020) Adulterants in selected dietary supplements and their detection methods. Drug Testing and Analysis 12:7, pages 861-886.
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Shi Shi, Yuanyang Wu, Minghao Zhou & Qiaoyuan Cheng. (2020) Simultaneous analysis of 31 anti-impotence compounds potentially illegally added to herbal-based dietary supplements by ultra-high-performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometry. Journal of Chromatography B 1144, pages 122077.
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Yogini S. Jaiswal & Leonard L. Williams. 2020. Herbal Medicine in India. Herbal Medicine in India 249 261 .
Sara S Mourad, Eman I El-Kimary, Magda A Barary & Dalia A Hamdy. (2019) Pharmacokinetic interaction between linagliptin and tadalafil in healthy Egyptian males using a novel LC–MS method. Bioanalysis 11:14, pages 1321-1336.
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Monika Jiru, Milena Stranska-Zachariasova, Zbynek Dzuman, Kamila Hurkova, Monika Tomaniova, Radim Stepan, Petr Cuhra & Jana Hajslova. (2019) Analysis of phosphodiesterase type 5 inhibitors as possible adulterants of botanical-based dietary supplements: extensive survey of preparations available at the Czech market. Journal of Pharmaceutical and Biomedical Analysis 164, pages 713-724.
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Elif Öztürk Er, Belma Özbek & Sezgin Bakırdere. (2018) A sensitive and selective analytical method for the simultaneous determination of sildenafil and tadalafil in water, energy drinks and sewage sludge matrices by LC-QTOF-MS/MS. Measurement 124, pages 64-71.
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Xiao-Bing Wang, Jing Zheng, Jun-Jie Li, Hai-Ying Yu, Qi-Yan Li, Li-Hua Xu, Ming-Jie Liu, Rui-Qing Xian, Yang-En Sun & Bing-Jie Liu. (2018) Simultaneous analysis of 23 illegal adulterated aphrodisiac chemical ingredients in health foods and Chinese traditional patent medicines by ultrahigh performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometry. Journal of Food and Drug Analysis 26:3, pages 1138-1153.
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A. Hemdan & Shereen M. Tawakol. (2018) HPLC–UV Chromatographic Methods for Detection and Quantification of Undeclared Withdrawn Synthetic Medications in Counterfeit Herbal Medicines with Confirmation by HPLC–PDA and Mass Spectrometry. Chromatographia 81:5, pages 777-783.
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Krystyna Skalicka-Woźniak, Milen I. Georgiev & Ilkay Erdogan Orhan. (2017) Adulteration of herbal sexual enhancers and slimmers: The wish for better sexual well-being and perfect body can be risky. Food and Chemical Toxicology 108, pages 355-364.
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Mark Avigan, Robert Mozersky & Leonard Seeff. (2016) Scientific and Regulatory Perspectives in Herbal and Dietary Supplement Associated Hepatotoxicity in the United States. International Journal of Molecular Sciences 17:3, pages 331.
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Ilkay Erdogan Orhan, Fatma Sezer Senol, Krystyna Skalicka-Wozniak, Milen Georgiev & Bilge Sener. 2016. Nutraceuticals. Nutraceuticals 153 182 .
Zhe Wang, Caisheng Wu, Gangli Wang, Qingsheng Zhang & Jinlan Zhang. (2015) Novel strategy for the determination of illegal adulterants in health foods and herbal medicines using high-performance liquid chromatography with high-resolution mass spectrometry. Journal of Separation Science 38:6, pages 925-935.
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Yolanda Picó. 2015. Advanced Mass Spectrometry for Food Safety and Quality. Advanced Mass Spectrometry for Food Safety and Quality 77 129 .
Lukas Vaclavik, Alexander J. Krynitsky & Jeanne I. Rader. (2014) Mass spectrometric analysis of pharmaceutical adulterants in products labeled as botanical dietary supplements or herbal remedies: a review. Analytical and Bioanalytical Chemistry 406:27, pages 6767-6790.
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Feng Shi, Changchuan Guo, Liping Gong, Jun Li, Peng Dong, Jinling Zhang, Ping Cui, Shuyin Jiang, Yanxia Zhao & Su Zeng. (2014) Application of a high resolution benchtop quadrupole-Orbitrap mass spectrometry for the rapid screening, confirmation and quantification of illegal adulterated phosphodiesterase-5 inhibitors in herbal medicines and dietary supplements. Journal of Chromatography A 1344, pages 91-98.
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Fenhong Song, Douglas Monroe, Aref El-Demerdash & Cynthia Palmer. (2014) Screening for multiple weight loss and related drugs in dietary supplement materials by flow injection tandem mass spectrometry and their confirmation by liquid chromatography tandem mass spectrometry. Journal of Pharmaceutical and Biomedical Analysis 88, pages 136-143.
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Yan Ren, Caisheng Wu & Jinlan Zhang. (2012) Simultaneous screening and determination of 18 illegal adulterants in herbal medicines and health foods for male sexual potency by ultra‐fast liquid chromatography‐electrospray ionization tandem mass spectrometry. Journal of Separation Science 35:21, pages 2847-2857.
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B.J. Venhuis & D. de Kaste. (2012) Towards a decade of detecting new analogues of sildenafil, tadalafil and vardenafil in food supplements: A history, analytical aspects and health risks. Journal of Pharmaceutical and Biomedical Analysis 69, pages 196-208.
Crossref
Etil Ariburnu, Mehmet Fazli Uludag, Huseyin Yalcinkaya & Erdem Yesilada. (2012) Comparative determination of sibutramine as an adulterant in natural slimming products by HPLC and HPTLC densitometry. Journal of Pharmaceutical and Biomedical Analysis 64-65, pages 77-81.
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