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Food Additives & Contaminants: Part A Volume 29, 2012 - Issue 4: Ministério da Agricultura, Pecuária e Abastecimento do Brasil – Laboratórios Nacionais Agropecuários: Methods of analysis for residues and contaminants in the food chain
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Original Articles

A multi-residue method for the determination of 90 pesticides in matrices with a high water content by LC–MS/MS without clean-up

Fernando Diniz Madureira Ministry of Agriculture, Livestock and Food Supply of Brazil, Laboratório Nacional Agropecuário (LANAGRO/MG), Pesticide Laboratory, Av. Rômulo Joviano, s/n Pedro Leopoldo, MG 33600-000, BrazilCorrespondence[email protected]
,
Fabiano Aurélio da Silva Oliveira Ministry of Agriculture, Livestock and Food Supply of Brazil, Laboratório Nacional Agropecuário (LANAGRO/MG), Pesticide Laboratory, Av. Rômulo Joviano, s/n Pedro Leopoldo, MG 33600-000, Brazil
,
Wesley Robert de Souza Ministry of Agriculture, Livestock and Food Supply of Brazil, Laboratório Nacional Agropecuário (LANAGRO/MG), Pesticide Laboratory, Av. Rômulo Joviano, s/n Pedro Leopoldo, MG 33600-000, Brazil
,
Ana Paula Pontelo Ministry of Agriculture, Livestock and Food Supply of Brazil, Laboratório Nacional Agropecuário (LANAGRO/MG), Pesticide Laboratory, Av. Rômulo Joviano, s/n Pedro Leopoldo, MG 33600-000, Brazil
,
Mauro Lúcio Gonçalves de Oliveira Ministry of Agriculture, Livestock and Food Supply of Brazil, Laboratório Nacional Agropecuário (LANAGRO/MG), Pesticide Laboratory, Av. Rômulo Joviano, s/n Pedro Leopoldo, MG 33600-000, Brazil
&
Gilsara Silva Ministry of Agriculture, Livestock and Food Supply of Brazil, Laboratório Nacional Agropecuário (LANAGRO/MG), Pesticide Laboratory, Av. Rômulo Joviano, s/n Pedro Leopoldo, MG 33600-000, Brazil
Pages 665-678 | Received 26 Nov 2010, Accepted 31 Aug 2011, Published online: 07 Nov 2011

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Jelmir Craveiro de Andrade, Diego Galvan, Luciane Effting, Letícia Tessaro, Adriano Aquino & Carlos Adam Conte-Junior. (2023) Multiclass Pesticide Residues in Fruits and Vegetables from Brazil: A Systematic Review of Sample Preparation Until Post-Harvest. Critical Reviews in Analytical Chemistry 53:6, pages 1174-1196.
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Nho-Eul Song, Dan-Bi Kim, Tae-Gyu Lim, Yun-Yeol Lee, Miyoung Yoo & Tae Gyu Nam. (2019) Determining pesticide residues in wheat flour by ultrahigh-performance liquid chromatography/quadrupole time-of-flight mass spectrometry with QuEChERS extraction. Food Additives & Contaminants: Part A 36:9, pages 1337-1347.
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Perihan Yolci Omeroglu, Árpad Ambrus & Dilek Boyacioglu. (2018) Uncertainty of pesticide residue concentration determined from ordinary and weighted linear regression curve. Food Additives & Contaminants: Part A 35:7, pages 1324-1339.
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Fabiano Aurélio da Silva Oliveira, Elba Nathália Corrêa Pereira, Jennifer Mattedi Gobbi, Benito Soto-Blanco & Marília Martins Melo. (2018) Multiresidue method for detection of pesticides in beef meat using liquid chromatography coupled to mass spectrometry detection (LC-MS) after QuEChERS extraction. Food Additives & Contaminants: Part A 35:1, pages 94-109.
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Articles from other publishers (15)

Aasma Bibi, Nazia Rafique, Sofia Khalid, Abdul Samad, Karam Ahad & Farrakh Mehboob. (2022) Method optimization and validation for the routine analysis of multi-class pesticide residues in Kinnow Mandarin and fruit quality evaluation. Food Chemistry 369, pages 130914.
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Weiguo Liu, Youzhi Su, Jun Liu, Kun Zhang, XiYuan Wang, Yinguang Chen, Luchun Duan & Feng Shi. (2021) Determination of cyflufenamid residues in 12 foodstuffs by QuEChERS-HPLC-MS/MS. Food Chemistry 362, pages 130148.
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Carolina de Gouveia M. D. E. Pinheiro, Fabiano Aurélio D. S. Oliveira, Silvia Catarina S. Oloris, Jean Berg A. da Silva & Benito Soto-Blanco. (2020) Pesticide Residues in Honey from Stingless Bee Melipona Subnitida (Meliponini, Apidae) . Journal of Apicultural Science 64:1, pages 29-36.
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Kukowski Klara, Gysbers Brianna, Stephen Fisher & Alena Kubátová. (2019) Optimization of Electrospray Ionization for Liquid Chromatography Time-of-Flight Mass Spectrometry Analysis of Preservatives in Wood Leachate Matrix. Chromatographia 82:11, pages 1677-1685.
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S Venu, K Santhi, Ashish Rawson, R Paranthaman & K Sureshkumar. (2019) Liquid chromatography–mass spectrometry/mass spectrometry method development for the determination of carbaryl residue in honey. Pharmacognosy Magazine 15:64, pages 205.
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Niharika Anand, Abhishek Kundu & Sujata Ray. (2017) A Validated Method for the Determination of Neonicotinoid, Pyrethroid and Organochlorine Residues in Human Milk. Chromatographia 81:2, pages 315-325.
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Federica Bianchi, Nicolò Riboni, Veronica Termopoli, Lucia Mendez, Isabel Medina, Leopold Ilag, Achille Cappiello & Maria Careri. (2018) MS-Based Analytical Techniques: Advances in Spray-Based Methods and EI-LC-MS Applications. Journal of Analytical Methods in Chemistry 2018, pages 1-24.
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Konstantinos M. Kasiotis, Angelos N. Tsakirakis, C. Richard Glass, Agathi N. Charistou, Pelagia Anastassiadou, Rianda Gerritsen-Ebben & Kyriaki Machera. (2017) Assessment of field re-entry exposure to pesticides: A dislodgeable foliar residue study. Science of The Total Environment 596-597, pages 178-186.
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Patrícia Amaral Souza Tette, Fabiano Aurélio da Silva Oliveira, Elba Nathália Corrêa Pereira, Gilsara Silva, Maria Beatriz de Abreu Glória & Christian Fernandes. (2016) Multiclass method for pesticides quantification in honey by means of modified QuEChERS and UHPLC–MS/MS. Food Chemistry 211, pages 130-139.
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V. G. Amelin & A. M. Andoralov. (2015) High-performance liquid chromatography–time-of-flight mass spectrometry in the identification and determination of 111 pesticides in food, feed, water, and soil. Journal of Analytical Chemistry 71:1, pages 82-93.
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Ajoy Saha, Ahammed Shabeer T. P.Kaushik Banerjee, Sandip Hingmire, Debarati Bhaduri, N. K. Jain & Sagar Utture. (2014) Simultaneous analysis of herbicides pendimethalin, oxyfluorfen, imazethapyr and quizalofop-p-ethyl by LC–MS/MS and safety evaluation of their harvest time residues in peanut (Arachis hypogaea L.). Journal of Food Science and Technology 52:7, pages 4001-4014.
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Anneli Kruve, Riin Rebane, Karin Kipper, Maarja-Liisa Oldekop, Hanno Evard, Koit Herodes, Pekka Ravio & Ivo Leito. (2015) Tutorial review on validation of liquid chromatography–mass spectrometry methods: Part II. Analytica Chimica Acta 870, pages 8-28.
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Claudia Oellig & Wolfgang Schwack. (2014) Planar solid phase extraction clean-up and microliter-flow injection analysis–time-of-flight mass spectrometry for multi-residue screening of pesticides in food. Journal of Chromatography A 1351, pages 1-11.
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María Castro-Puyana & Miguel Herrero. (2013) Metabolomics approaches based on mass spectrometry for food safety, quality and traceability. TrAC Trends in Analytical Chemistry 52, pages 74-87.
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Raphaella P. Carneiro, Fabiano A.S. Oliveira, Fernando D. Madureira, Gilsara Silva, Wesley R. de Souza & Renata Pereira Lopes. (2013) Development and method validation for determination of 128 pesticides in bananas by modified QuEChERS and UHPLC–MS/MS analysis. Food Control 33:2, pages 413-423.
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