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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 31, 2001 - Issue 13
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Original Articles

SOLVENT FREE BECKMANN REARRANGEMENT OF KETOXIMES BY ANHYDROUS FERRIC CHLORIDE

M. M. Khodaei Department of Chemistry, Razi University, Kermanshah, Iran
,
F. A. Meybodi Department of Phytochemistry, Medicinal Plants Research Institute, Shahid Beheshti University, Tehran, Iran
,
N. Rezai Department of Phytochemistry, Medicinal Plants Research Institute, Shahid Beheshti University, Tehran, Iran
&
P. Salehi Department of Phytochemistry, Medicinal Plants Research Institute, Shahid Beheshti University, Tehran, Iran
Pages 2047-2050 | Received 13 Sep 2000, Published online: 09 Nov 2006

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Rawesh Kumar, Sneha Shah, Prangya Paramita Das, Gami Girish Kumar Bhagavanbhai, Ahmed Al Fatesh & Biswajit Chowdhury. (2019) An overview of caprolactam synthesis. Catalysis Reviews 61:4, pages 516-594.
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Feng-Yu Piao, Yu-Zhong Xie, Wen-Bin Zhang, Wei Zhang & Rong-Bi Han. (2013) High-Yield Method for the Preparation of 1,3,4,5-Tetrahydro-7-methoxy-2H-1-benzazepin-2-one with Excellent Regio- and Stereoselectivity. Synthetic Communications 43:14, pages 1920-1930.
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Feng Xu, Ni-Ge Wang, You-Ping Tian, Yong-Mei Chen & Wei-Chun Liu. (2012) Ph3P/I2-Catalyzed Beckmann Rearrangement of Ketoximes into Amides. Synthetic Communications 42:23, pages 3532-3539.
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Hossein Eshghi & Asadollah Hassankhani. (2005) REGIOSELECTIVE SYNTHESIS OF E-OXIMES CATALYZED BY FERRIC CHLORIDE UNDER SOLVENT-FREE CONDITIONS. Organic Preparations and Procedures International 37:6, pages 575-579.
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Peyman Salehi, Mohammad Mahdi Khodaei, Mohammad Ali Zolfigol & Shahpour Zeinoldini. (2003) Catalytic Friedel–Crafts Acylation of Alkoxy Benzenes by Ferric Hydrogensulfate. Synthetic Communications 33:8, pages 1367-1373.
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Daniel M. Baier, Tilo Rensch, Desislava Dobreva, Carolina Spula, Stephen Fanenstich, Marisol Rappen, Konrad Bergheim, Sven Grätz & Lars Borchardt. (2022) The Mechanochemical Beckmann Rearrangement over Solid Acids: From the Ball Mill to the Extruder. Chemistry–Methods 3:4.
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Rita Mocci, Evelina Colacino, Lidia De Luca, Claudia Fattuoni, Andrea Porcheddu & Francesco Delogu. (2021) The Mechanochemical Beckmann Rearrangement: An Eco-efficient “Cut-and-Paste” Strategy to Design the “Good Old Amide Bond”. ACS Sustainable Chemistry & Engineering 9:5, pages 2100-2114.
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Jie Jack LiJie Jack Li. 2021. Name Reactions. Name Reactions 25 28 .
Kamalpreet Kaur & Suman Srivastava. (2020) Beckmann rearrangement catalysis: a review of recent advances. New Journal of Chemistry 44:43, pages 18530-18572.
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Sheena Mahajan, Bhavana Sharma & Kamal K. Kapoor. (2015) A solvent-free one step conversion of ketones to amides via Beckmann rearrangement catalysed by FeCl3·6H2O in presence of hydroxylamine hydrochloride. Tetrahedron Letters 56:14, pages 1915-1918.
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Rajesh G. Kalkhambkar & Hemantkumar M. Savanur. (2015) Highly efficient synthesis of amides from ketoximes using trifluoromethanesulphonic anhydride. RSC Advances 5:74, pages 60106-60113.
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Zvi RappoportM. Manuela A. Pereira & Pedro Paulo Santos. 2010. Patai's Chemistry of Functional Groups. Patai's Chemistry of Functional Groups.
Lal Dhar S. Yadav, Garima & Vishnu P. Srivastava. (2010) Bromodimethylsulfonium bromide (BDMS) in ionic liquid: a mild and efficient catalyst for Beckmann rearrangement. Tetrahedron Letters 51:4, pages 739-743.
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Jie Jack LiJie Jack Li. 2009. Name Reactions. Name Reactions 33 35 .
Koichi Tanaka. 2008. Solvent‐Free Organic Synthesis. Solvent‐Free Organic Synthesis 343 364 .
Hamid Reza Shaterian, Hossein Yarahmadi & Majid Ghashang. (2008) An efficient, simple and expedition synthesis of 1-amidoalkyl-2-naphthols as ‘drug like’ molecules for biological screening. Bioorganic & Medicinal Chemistry Letters 18:2, pages 788-792.
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Hossien A. Oskooie, Majid M. Heravi, Akbar Sadnia, Mehrak Safarzadegan & Farahnaz K. Behbahani. (2007) Mild and efficient conversion of oximes into arylhydrazones catalysed by ferric perchlorate. Mendeleev Communications 17:3, pages 190-191.
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Yasuhiro Torisawa, Takao Nishi & Jun-ichi Minamikawa. (2007) Continuing efforts on the improvement of Beckmann rearrangement of indanone oxime. Bioorganic & Medicinal Chemistry Letters 17:2, pages 448-452.
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Chun-Ming Ma, Peng-Zhi Zheng & Jian-Ping Li. (2006) Solid-State Synthesis and Characterization of 2-Thioxo-4-Imidazolidinone Derivatives. Journal of the Chinese Chemical Society 53:3, pages 633-636.
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Andrew D. White & Fabrice Gallou. 2001. Encyclopedia of Reagents for Organic Synthesis. Encyclopedia of Reagents for Organic Synthesis.
Mona Hosseini-Sarvari & Hashem Sharghi. (2019) Alumina Sulfuric Acid Mediated Solvent-Free and One-Step Beckmann Rearrangement of Ketones and Aldehydes and a Useful Reagent for Synthesis of Keto- and Ald-Oximes. Journal of Chemical Research 2006:3, pages 205-208.
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. 2006. Name Reactions. Name Reactions 41 42 .
Na Zhao & Yu-Lu Wang. (2019) A mild and simple synthesis of N -aryl substituted toluenesulfamides under solvent-free conditions . Journal of Chemical Research 2004:5, pages 366-367.
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Michael B. Smith. 2003. Compendium of Organic Synthetic Methods. Compendium of Organic Synthetic Methods 226 263 .
Yasuhiro Torisawa, Takao Nishi & Jun-ichi Minamikawa. (2003) A study on the conversion of indanones into carbostyrils. Bioorganic & Medicinal Chemistry 11:10, pages 2205-2209.
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Hashem Sharghi & Mona Hosseini Sarvari. (2019) Titanium Oxide (TiO 2 ) Catalysed One-Step Beckmann Rearrangement of Aldehydes and Ketones in Solvent Free Conditions . Journal of Chemical Research 2003:3, pages 176-178.
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Peyman Salehi, Minoo Dabiri, Mohammad Ali Zolfigol & Mohammad Ali Bodaghi Fard. (2003) Efficient Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones over Silica Sulfuric Acid as a Reusable Catalyst under Solvent-free Conditions. HETEROCYCLES 60:11, pages 2435.
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Jie Jack LiJie Jack Li. 2002. Name Reactions. Name Reactions 25 25 .
M. M. Khodaei, F. A. Meybodi, N. Rezai & P. Salehi. (2010) ChemInform Abstract: Solvent Free Beckmann Rearrangement of Ketoximes by Anhydrous Ferric Chloride.. ChemInform 32:47.
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