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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 34, 2004 - Issue 9
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Original Articles

Simple Protocol for the Synthesis of 3,4‐Dihydropyrimidin‐2(1H)‐ones Using SnCl2 · 2H2O–LiCl as an Inexpensive Catalyst System

M. Shailaja Organic Chemistry Division—II, Indian Institute of Chemical Technology, Hyderabad, 500007, India
,
A. Manjula Organic Chemistry Division—II, Indian Institute of Chemical Technology, Hyderabad, 500007, India
,
B. Vittal Rao Organic Chemistry Division—II, Indian Institute of Chemical Technology, Hyderabad, 500007, IndiaCorrespondence[email protected]
&
Neelakantan Parvathi Organic Chemistry Division—II, Indian Institute of Chemical Technology, Hyderabad, 500007, India
Pages 1559-1564 | Received 25 Oct 2002, Published online: 16 Aug 2006

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Sharmil N. Anjirwala, Parnas S. Parmar & Saurabh K. Patel. (2022) Synthetic protocols for non-fused pyrimidines. Synthetic Communications 52:22, pages 2079-2121.
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AbdolR. Hajipour & Mohadeseh Seddighi. (2012) Pyridinium-Based Brønsted Acidic Ionic Liquid as a Highly Efficient Catalyst for One-Pot Synthesis of Dihydropyrimidinones. Synthetic Communications 42:2, pages 227-235.
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Min Wang, Heng Jiang, Zhiguo Song & Hong Gong. (2009) Copper Nitrate Catalyzed Three-Component One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1H)-Ones. Preparative Biochemistry & Biotechnology 39:4, pages 372-379.
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M. Syamala. (2009) Recent Progress in Three-Component Reactions. An Update. Organic Preparations and Procedures International 41:1, pages 1-68.
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Hanane El Badaoui, Fathallaah Bazi, Soumia Tamani, Saïd Boulaajaj, Mohamed Zahouily, Hassan B. Lazrek & Saïd Sebti. (2005) Lewis Acid–Doped Natural Phosphate: New Catalysts for the One‐Pot Synthesis of 3,4‐Dihydropyrimdin‐2(1H)‐one. Synthetic Communications 35:19, pages 2561-2568.
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Vincent Escande, Laetitia Garoux, Claire Grison, Yann Thillier, Françoise Debart, Jean-Jacques Vasseur, Clothilde Boulanger & Claude Grison. (2014) Ecological catalysis and phytoextraction: Symbiosis for future. Applied Catalysis B: Environmental 146, pages 279-288.
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Dmitriy M. Volochnyuk, Oleksandr O. Grygorenko & Alina O. Gorlova. 2014. Fluorine in Heterocyclic Chemistry Volume 2. Fluorine in Heterocyclic Chemistry Volume 2 291 575 .
Kawaljit Singh & Kamaljit Singh. 2012. 223 308 .
Hemant S. Chandak, Nitin P. Lad & Pravin P. Upare. (2009) Recyclable Amberlyst-70 as a Catalyst for Biginelli Reaction: An Efficient One-Pot Green Protocol for the Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones. Catalysis Letters 131:3-4, pages 469-473.
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Maksim A. Kolosov, Valeriy D. Orlov, Dmitriy A. Beloborodov & Victor V. Dotsenko. (2008) A chemical placebo: NaCl as an effective, cheapest, non-acidic and greener catalyst for Biginelli-type 3,4-dihydropyrimidin-2(1H)-ones (-thiones) synthesis. Molecular Diversity 13:1, pages 5-25.
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Pranav Kumar, Ashutosh Kumar, Shyam Sundar Verma, Namrata Dwivedi, Nasib Singh, Mohammad Imran Siddiqi, Rama Pati Tripathi, Anuradha Dube & Neeloo Singh. (2008) Leishmania donovani pteridine reductase 1: Biochemical properties and structure-modeling studies. Experimental Parasitology 120:1, pages 73-79.
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Sergey V. Ryabukhin, Andrey S. Plaskon, Eugeniy N. Ostapchuk, Dmitriy M. Volochnyuk, Oleg V. Shishkin & Andrey A. Tolmachev. (2008) CF3-substituted 1,3-dicarbonyl compounds in the Biginelli reaction promoted by chlorotrimethylsilane. Journal of Fluorine Chemistry 129:7, pages 625-631.
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Ch. Sanjeeva Reddy & A. Nagaraj. (2007) ZIRCONIUM OXYCHLORIDE AS A NEW AND EFFICIENT CATALYST FOR THE SYNTHESIS OF 3,4-DIHYDROPYRIMIDINE-2(1H)- THIONE/ONE UNDER SOLVENT-FREE MICROWAVE IRRADIATION CONDITIONS. Heterocyclic Communications 13:1.
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Margaret M. Faul & Oliver R. Thiel. 2001. Encyclopedia of Reagents for Organic Synthesis. Encyclopedia of Reagents for Organic Synthesis.
R. A. Stockman. (2005) 4  Heterocyclic chemistry. Annual Reports Section "B" (Organic Chemistry) 101, pages 103.
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M. Shailaja, A. Manjula, B. Vittal Rao & Neelakantan Parvathi. (2004) Simple Protocol for the Synthesis of 3,4‐Dihydropyrimidin‐2(1H)‐ones Using SnCl 2 ×2H 2 O—LiCl as an Inexpensive Catalyst System. . ChemInform 35:40.
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