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Science and Technology of Advanced Materials Volume 16, 2015 - Issue 2

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Preparation of macroporous zirconia monoliths from ionic precursors via an epoxide-mediated sol-gel process accompanied by phase separation

Xingzhong GuoSchool of Materials Science and Engineering, Zhejiang University, Hangzhou, 310027, People’s Republic of ChinaCorrespondence[email protected] (X Guo)

Jie SongSchool of Materials Science and Engineering, Zhejiang University, Hangzhou, 310027, People’s Republic of China

Yixiu LvlinSchool of Materials Science and Engineering, Zhejiang University, Hangzhou, 310027, People’s Republic of China

Kazuki NakanishiDepartment of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa, Sakyo-ku, Kyoto606-8502, Japan

Kazuyoshi KanamoriDepartment of Chemistry, Graduate School of Science, Kyoto University, Kitashirakawa, Sakyo-ku, Kyoto606-8502, Japan

Hui YangSchool of Materials Science and Engineering, Zhejiang University, Hangzhou, 310027, People’s Republic of ChinaCorrespondence[email protected]

Article: 025003 | Received 22 Dec 2014, Accepted 24 Feb 2015, Published online: 23 Mar 2015

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https://doi.org/10.1088/1468-6996/16/2/025003
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Yuji Sato, Kazuyoshi Kanamori & Kazuki Nakanishi. (2023) Preparation of Hierarchically Porous Niobium(V) Oxide and Alkaline Niobate Monoliths via Sol–Gel Accompanied by Phase Separation. Chemistry of Materials 35:13, pages 5177-5184.
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Xuanming Lu & Kazuki Nakanishi. (2021) Synthesis of Hierarchically Porous Metal Oxide Monoliths via Sol–Gel Process Accompanied by Phase Separation From Divalent Metal Salts: A Short Review. Frontiers in Chemical Engineering 3.
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Ana C. Marques & Mário Vale. (2021) Macroporosity Control by Phase Separation in Sol-Gel Derived Monoliths and Microspheres. Materials 14:15, pages 4247.
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Xuanming Lu, Kazuyoshi Kanamori, George Hasegawa & Kazuki Nakanishi. (2021) Preparation of hierarchically porous spinel CoMn 2 O 4 monoliths via sol–gel process accompanied by phase separation . Journal of the American Ceramic Society 104:6, pages 2449-2459.
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Xuanming Lu, Kazuyoshi Kanamori & Kazuki Nakanishi. (2020) Hierarchically porous monoliths based on low-valence transition metal (Cu, Co, Mn) oxides: gelation and phase separation. National Science Review 7:11, pages 1656-1666.
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Fan Wang, Yukun Sun, Xingzhong Guo, Dongyun Li & Hui Yang. (2020) Preparation and graft modification of hierarchically porous ferriferrous oxide for heavy metal ions adsorption. Journal of Sol-Gel Science and Technology 96:2, pages 360-369.
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Shengfei Li, Mingchun Li, Aili Tao, Minggao Song, Baoting Wang, Jiaming Niu, Fuyuan Yu & Yusheng Wu. (2020) Synthesis of a bicontinuous structured SrTiO3 porous film with significant photocatalytic activity by controlling phase separation process. Journal of Sol-Gel Science and Technology 94:2, pages 288-297.
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Fei Li, Xin-Gang Wang, Xiao Huang, Ji-Xuan Liu, Weichao Bao, Guo-Jun Zhang & Hongzhi Wang. (2018) Preparation of ZrC/SiC porous self-supporting monoliths via sol-gel process using polyethylene glycol as phase separation inducer. Journal of the European Ceramic Society 38:14, pages 4806-4813.
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Andrea Feinle, Michael S. Elsaesser & Nicola Hüsing. 2018. Handbook of Sol-Gel Science and Technology. Handbook of Sol-Gel Science and Technology 867 915 .

Y. J. Wu, W. T. Zhang, M. M. Yang, Y. H. Zhao, Z. T. Liu & J. Y. Yan. (2017) Cobalt supported on Zr-modified SiO 2 as an efficient catalyst for Fischer–Tropsch synthesis . RSC Advances 7:39, pages 24157-24162.
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Mingliang Sun, Tianbo Zhao, Zunfeng Li, Zhaofei Ma, Jia Wang & Fengyan Li. (2016) Sol-gel synthesis of macro-mesoporous Al2O3-SiO2-TiO2 monoliths via phase separation route. Ceramics International 42:14, pages 15926-15932.
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Xingzhong Guo, Qilong Zhang, Xingeng Ding, Qianhong Shen, Chunchun Wu, Lingjie Zhang & Hui Yang. (2016) Synthesis and application of several sol–gel-derived materials via sol–gel process combining with other technologies: a review. Journal of Sol-Gel Science and Technology 79:2, pages 328-358.
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Xingzhong Guo, Jie Song, Jing Ren, Fanger Yang, Kazuyoshi Kanamori & Kazuki Nakanishi. (2016) Facile preparation of well-defined macroporous yttria-stabilized zirconia monoliths via sol–gel process accompanied by phase separation. Journal of Porous Materials 23:4, pages 867-875.
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Jing Li, Tianbo Zhao, Fengyan Li, Baoning Zong, Zexue Du & Jianli Zeng. (2016) A comparative study on the synthesis mechanism and microstructural development of hierarchical porous mullite monoliths obtained by the sol–gel process with three different silicon sources. Ceramics International 42:4, pages 4806-4818.
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A. Feinle, M. S. Elsaesser & N. Hüsing. (2016) Sol–gel synthesis of monolithic materials with hierarchical porosity. Chemical Society Reviews 45:12, pages 3377-3399.
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V.V. Ranade & S.S. Joshi. 2016. Industrial Catalytic Processes for Fine and Specialty Chemicals. Industrial Catalytic Processes for Fine and Specialty Chemicals 1 14 .

Andrea Feinle, Michael S. Elsaesser & Nicola Hüsing. 2016. Handbook of Sol-Gel Science and Technology. Handbook of Sol-Gel Science and Technology 1 49 .

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Preparation of macroporous zirconia monoliths from ionic precursors via an epoxide-mediated sol-gel process accompanied by phase separation

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Preparation of macroporous zirconia monoliths from ionic precursors via an epoxide-mediated sol-gel process accompanied by phase separation

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