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Advances in Applied Ceramics
Structural, Functional and Bioceramics
Volume 105, 2006 - Issue 4: Advances in cement and concrete science
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Articles

In situ Raman analysis of hydrating C3A and C4AF pastes in presence and absence of sulphate

L. BlackMaterials & Engineering Research Institute, Sheffield Hallam University, Howard Street, Sheffield, S1 1WB, UKCorrespondence[email protected]
,
C. BreenMaterials & Engineering Research Institute, Sheffield Hallam University, Howard Street, Sheffield, S1 1WB, UK
,
J. YarwoodMaterials & Engineering Research Institute, Sheffield Hallam University, Howard Street, Sheffield, S1 1WB, UK
,
J. PhippsSchlumberger Cambridge Research, High Cross, Madingley, Cambridge, CB3 0EL, UK
&
G. MaitlandDepartment of Chemical Engineering, Imperial College London, South Kensington Campus, London, SW7 2AZ, UK
Pages 209-216 | Published online: 18 Jul 2013

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Vincent Cantarel & Isao Yamagishi. (2022) Geopolymer and ordinary Portland cement interface analyzed by micro-Raman and SEM. Journal of Nuclear Science and Technology 59:7, pages 888-897.
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Leon Black, Phil Purnell & Joanne Hill. (2010) Current themes in cement research. Advances in Applied Ceramics 109:5, pages 253-259.
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E Dubina, L Black, R Sieber & J Plank. (2010) Interaction of water vapour with anhydrous cement minerals. Advances in Applied Ceramics 109:5, pages 260-268.
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L. Black & A. Brooker. (2007) SEM–SCA: combined SEM – Raman spectrometer for analysis of OPC clinker. Advances in Applied Ceramics 106:6, pages 327-334.
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Emmanuel Safari Leo, Mark G. Alexander & Hans Beushausen. (2023) Optimisation of mix proportions of LC3 binders with African clays, based on compressive strength of mortars, and associated hydration aspects. Cement and Concrete Research 173, pages 107255.
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Nicolas Bulidon, Krystel Pelissier, Clément Boissy, Christophe Mendibide, Valérie Maillot, Xavier Bourbon & Didier Crusset. (2023) Hydrogen production through aluminium corrosion in a cement‐based matrix. Materials and Corrosion 74:11-12, pages 1765-1776.
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Jiangchuan Li, Tian Zeng & Jun Chang. (2023) Microstructure of Fe(OH)3 phase in hydration products of calcium sulfoaluminate cement. Construction and Building Materials 400, pages 132609.
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Nan Yang, Aihong Li, Qing Liu, Yanshuai Cui, Zhaojia Wang, Yukun Gao & Jianping Guo. (2023) Incorporation and solidification mechanism of manganese doped cement clinker. Frontiers in Chemistry 11.
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Konstantinos Sotiriadis, Radosław Mróz, Petra Mácová, Anton S. Mazur & Andraž Krajnc. (2022) Long-term sulfate resistance of synthesized cement systems with variable C3A/C4AF ratio at low temperature or ambient conditions: Insights into the crystalline and amorphous phase assemblage. Cement and Concrete Research 160, pages 106902.
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K. Snehal, BB Das & Salim Barbhuiya. (2022) Influence of aggressive exposure on the degradation of nano-silica admixed cementitious mortar integrated with phase change materials. Construction and Building Materials 335, pages 127467.
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Sinje Zimmer, Johannes Kehren, Lee Klein, Florian Holleyn & Olaf Krause. (2022) Raman-Spektroskopie ermöglicht neue Einblicke in die keramische Welt. Keramische Zeitschrift 74:3, pages 48-55.
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Bingrong Li, Yaowu Wei, Junfeng Chen & Nan Li. (2022) Influence of tricalcium aluminate on the microstructure evolution of CaO specimen during hydration. Journal of the European Ceramic Society 42:4, pages 1796-1803.
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Gaoyin Zhang, Zhiqiang Wu, Xiaowei Cheng, Xialan Sun, Chunmei Zhang & Ming Zhou. (2022) Mechanical properties of high-ferrite oil-well cement used in shale gas horizontal wells under various loads. Construction and Building Materials 319, pages 126067.
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J Pauli, A Ramírez, C Crasselt, W Schmidt & U Resch-Genger. (2021) Utilizing optical spectroscopy and 2′,7′-difluorofluorescein to characterize the early stages of cement hydration. Methods and Applications in Fluorescence 10:1, pages 015001.
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Yongqiang Li, Tangwei Mi, Xiaobo Ding, Wei Liu, Biqin Dong, Zhijun Dong, Luping Tang & Feng Xing. (2022) Assessment of compositional changes of carbonated cement pastes subjected to high temperatures using in-situ Raman mapping and XPS. Journal of Building Engineering 45, pages 103454.
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Jiangwei Xue, Songhui Liu, Xiaoe Ma, Yibiao Teng & Xuemao Guan. (2022) Effect of different gypsum dosage on the chloride binding properties of C4AF hydrated paste. Construction and Building Materials 315, pages 125562.
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M Krejcí Kotlanova & V Masek. (2021) Raman spectroscopy of interfacial transition zone in concrete doped with limestone powder and metakaolin. IOP Conference Series: Materials Science and Engineering 1039:1, pages 012003.
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Gaoyin Zhang, Qiang Ren, Jianyong He, Shiwei Jiang, Xiaowei Cheng, Yang Yu, Sheng Huang, Chunmei Zhang & Ming Zhou. (2021) New understanding of early hydration of C4AF under surface vitrification. Powder Technology 377, pages 372-378.
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Lin Sha, Zhemin Zou, Jun Qu, Xinfei Li, Yiyi Huang, Chenjie Wu & Zhigao Xu. (2020) As(III) removal from aqueous solution by katoite (Ca3Al2(OH)12). Chemosphere 260, pages 127555.
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Ping Chen, Shuming Zhang, Huamei Yang & Cheng Hu. (2019) Effects of Curing Temperature on Rheological Behaviour and Compressive Strength of Cement Containing GGBFS. Journal of Wuhan University of Technology-Mater. Sci. Ed. 34:5, pages 1155-1162.
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Xiao Huang, Fazhou Wang, Shuguang Hu, Yang Lu, Meijuan Rao & Yuandong Mu. (2019) Brownmillerite hydration in the presence of gypsum: The effect of Al/Fe ratio and sulfate ions. Journal of the American Ceramic Society 102:9, pages 5545-5554.
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Yanfei Yue, Jing Jing Wang, P.A. Muhammed Basheer, John J. Boland & Yun Bai. (2018) A Raman spectroscopy based optical fibre system for detecting carbonation profile of cementitious materials. Sensors and Actuators B: Chemical 257, pages 635-649.
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Yanfei Yue, Jing Jing Wang, P.A. Muhammed Basheer & Yun Bai. (2018) Raman spectroscopic investigation of Friedel's salt. Cement and Concrete Composites 86, pages 306-314.
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Yanfei Yue, Jing Jing Wang, P.A. Muhammed Basheer, John J. Boland & Yun Bai. (2017) Characterisation of carbonated Portland cement paste with optical fibre excitation Raman spectroscopy. Construction and Building Materials 135, pages 369-376.
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Héctor Morillas, Javier García-Galan, Maite Maguregui, Cristina García-Florentino, Iker Marcaida, Jose Antonio Carrero & Juan Manuel Madariaga. (2016) In-situ multianalytical methodology to evaluate the conservation state of the entrance arch of La Galea Fortress (Getxo, north of Spain). Microchemical Journal 128, pages 288-296.
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E. Dubina, J. Plank & L. Black. (2015) Impact of water vapour and carbon dioxide on surface composition of C3A polymorphs studied by X-ray photoelectron spectroscopy. Cement and Concrete Research 73, pages 36-41.
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Ray L. Frost, Andrés López, Lina Wang, Antônio Wilson Romano & Ricardo Scholz. (2015) A vibrational spectroscopic study of the silicate mineral harmotome – (Ba,Na,K)1-2(Si,Al)8O16⋅6H2O – A natural zeolite. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 137, pages 70-74.
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Ray L. Frost, Andrés López, Frederick L. Theiss, Antônio Wilson Romano & Ricardo Scholz. (2015) A vibrational spectroscopic study of the silicate mineral pectolite – NaCa2Si3O8(OH). Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 134, pages 58-62.
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Hugh Wang, Delia De Leon & Hamid Farzam. (2014) C 4 AF Reactivity—Chemistry and Hydration of Industrial Cement . ACI Materials Journal 111:2.
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D. Ectors, J. Neubauer & F. Goetz-Neunhoeffer. (2013) The hydration of synthetic brownmillerite in presence of low Ca-sulfate content and calcite monitored by quantitative in-situ-XRD and heat flow calorimetry. Cement and Concrete Research 54, pages 61-68.
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David Torréns-Martín, Lucia Fernández-Carrasco, Sagrario Martínez-Ramírez, Jordi Ibáñez, Lluis Artús & Thomas Matschei. (2013) Raman Spectroscopy of Anhydrous and Hydrated Calcium Aluminates and Sulfoaluminates. Journal of the American Ceramic Society 96:11, pages 3589-3595.
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Nishant Garg, Kejin Wang & Steve W. Martin. (2013) A Raman spectroscopic study of the evolution of sulfates and hydroxides in cement–fly ash pastes. Cement and Concrete Research 53, pages 91-103.
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Thomas Schmid & Petra Dariz. (2013) Determination and imaging of binder remnants and aggregates in historic cement stone by Raman microscopy. Journal of Raman Spectroscopy 44:6, pages 882-891.
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David Torréns-Martín, Lucia Fernández-Carrasco & Sagrario Martínez-Ramírez. (2013) Hydration of calcium aluminates and calcium sulfoaluminate studied by Raman spectroscopy. Cement and Concrete Research 47, pages 43-50.
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Ray L. Frost, Mahen Mahendran, Keerthan Poologanathan & Yunfei Xi. (2012) Raman spectroscopic study of the mineral xonotlite Ca6Si6O17(OH)2—A component of plaster boards. Materials Research Bulletin 47:11, pages 3644-3649.
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M. Chollet & M. Horgnies. (2011) Analyses of the surfaces of concrete by Raman and FT-IR spectroscopies: comparative study of hardened samples after demoulding and after organic post-treatment. Surface and Interface Analysis 43:3, pages 714-725.
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Sagrario Martínez-Ramírez & Moisés Frias. (2011) Micro-Raman study of stable and metastable phases in metakaolin/Ca(OH)2 system cured at 60°C. Applied Clay Science 51:3, pages 283-286.
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I.G. Richardson, J. Skibsted, L. Black & R.J. Kirkpatrick. (2010) Characterisation of cement hydrate phases by TEM, NMR and Raman spectroscopy. Advances in Cement Research 22:4, pages 233-248.
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Göril Möschner, Barbara Lothenbach, Frank Winnefeld, Andrea Ulrich, Renato Figi & Ruben Kretzschmar. (2009) Solid solution between Al-ettringite and Fe-ettringite (Ca6[Al1−xFex(OH)6]2(SO4)3·26H2O). Cement and Concrete Research 39:6, pages 482-489.
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Robert Ianoş. (2011) An efficient solution for the single-step synthesis of 4CaO·Al 2 O 3 ·Fe 2 O 3 powders . Journal of Materials Research 24:1, pages 245-252.
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D. Gastaldi, E. Boccaleri & F. Canonico. (2008) In situ Raman study of mineral phases formed as by‐products in a rotary kiln for clinker production . Journal of Raman Spectroscopy 39:7, pages 806-812.
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Daniela Gastaldi, Enrico Boccaleri, Fulvio Canonico & Manuela Bianchi. (2007) The use of Raman spectroscopy as a versatile characterization tool for calcium sulphoaluminate cements: a compositional and hydration study. Journal of Materials Science 42:20, pages 8426-8432.
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Leon Black, Chris Breen, Jack Yarwood, Krassimir Garbev, Peter Stemmermann & Biliana Gasharova. (2007) Structural Features of C–S–H(I) and Its Carbonation in Air—A Raman Spectroscopic Study. Part II: Carbonated Phases. Journal of the American Ceramic Society 90:3, pages 908-917.
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Guillaume RenaudinRachid SegniDorota MentelJean-Marie NedelecFabrice LerouxChristine Taviot-Gueho. (2007) A Raman Study of the Sulfated Cement Hydrates: Ettringite and Monosulfoaluminate. Journal of Advanced Concrete Technology 5:3, pages 299-312.
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