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Future Science OA Volume 7, 2021 - Issue 10

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Commentary

The Critical Role of Mobile Phase pH in the Performance of Oligonucleotide Ion-Pair Liquid Chromatography–Mass Spectrometry Methods

Guilherme J Guimaraes1 Department of Pharmaceutical & Biomedical Sciences, College of Pharmacy, University of Georgia, Athens, GA, USA

https://orcid.org/0000-0001-7778-4905

Michael G Bartlett1 Department of Pharmaceutical & Biomedical Sciences, College of Pharmacy, University of Georgia, Athens, GA, USACorrespondence[email protected]

https://orcid.org/0000-0003-0626-3234

Article: FSO753 | Received 13 Jul 2021, Accepted 29 Sep 2021, Published online: 23 Oct 2021

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https://doi.org/10.2144/fsoa-2021-0084
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Jennifer L. Lippens, Heath C. Timmons, Crystal Welch, Aditya Kulkarni & Tawnya G. Flick. (2023) Rapid Intact Mass Analysis and Evaluation of the Separation Potential of Microfluidic Capillary Electrophoresis Mass Spectrometry for Oligonucleotides. Journal of the American Society for Mass Spectrometry 34:11, pages 2491-2497.
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Aowen Liu, Ming Cheng, Yixuan Zhou & Pan Deng. (2022) Bioanalysis of Oligonucleotide by LC–MS: Effects of Ion Pairing Regents and Recent Advances in Ion-Pairing-Free Analytical Strategies. International Journal of Molecular Sciences 23:24, pages 15474.
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Sylwia Studzińska, Feiyang Li, Michał Szumski, Bogusław Buszewski & Michael Lämmerhofer. (2022) Cholesterol Stationary Phase in the Separation and Identification of siRNA Impurities by Two-Dimensional Liquid Chromatography-Mass Spectrometry. International Journal of Molecular Sciences 23:23, pages 14960.
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Fabien Hannauer, Rachelle Black, Andrew D. Ray, Eugen Stulz, G. John Langley & Stephen W. Holman. (2022) Advancements in the characterisation of oligonucleotides by high performance liquid chromatography‐mass spectrometry in 2021: A short review. Analytical Science Advances 3:3-4, pages 90-102.
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