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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 194, 2019 - Issue 4-6: Proceedings of the 2018 International Conference on Phosphorus Chemistry, ICPC-22
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Original Articles

Synthesis and characterization of poly([Eu or Dy] 1,1’-ferrocenediyl-bis(H-phosphinates))

R. P. ShekurovArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaORCID Iconhttp://orcid.org/0000-0002-2203-6675View further author information
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L. H. GilmanovaArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaORCID Iconhttp://orcid.org/0000-0002-0344-6919View further author information
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M. N. KhrizanforovArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaORCID Iconhttp://orcid.org/0000-0003-4714-4143View further author information
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S. O. StrekalovaArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaCorrespondence[email protected]
ORCID Iconhttp://orcid.org/0000-0002-7940-7895View further author information
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Y. H. BudnikovaArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaORCID Iconhttp://orcid.org/0000-0001-9497-4006View further author information
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T. P. GerasimovaArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaORCID Iconhttp://orcid.org/0000-0001-8473-5327View further author information
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S. A. KatsyubaArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaORCID Iconhttp://orcid.org/0000-0001-9196-9308View further author information
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V. A. MiluykovArbuzov Institute of Organic and Physical Chemistry, FRC Kazan Scientific Center of RAS, Kazan, RussiaORCID Iconhttp://orcid.org/0000-0002-8069-457XView further author information
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Pages 459-462 | Received 27 Sep 2018, Accepted 17 Oct 2018, Published online: 17 Feb 2019
 
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Abstract

Metal-organic frameworks [M2L3]n have been synthesized using ferrocene-based ligand bearing phosphinic groups L = 1,1’-ferrocenediyl-bis(H-phosphinic acid)) and M(III) = Eu, Dy. Structures of complexes 1 and 2 are studied by IR and powder XRD analyses and shown to be isomorphic. The thermal decomposition of the synthesized compounds was studied by differential scanning calorimetry and thermogravimetry.

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Additional information

Funding

This research was supported by the Russian Foundation for Basic Research and the government of the Tatarstan Republic, grant No 18-43-160014.

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