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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 198, 2023 - Issue 5
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Research articles

An efficient one-pot synthesis of highly functionalized selenophenes

Zeinab Vojdania Department of Chemistry, Yazd Branch, Islamic Azad University, Yazd, Iran
,
Mohammad H. Mosslemina Department of Chemistry, Yazd Branch, Islamic Azad University, Yazd, IranCorrespondence[email protected]
ORCID Iconhttps://orcid.org/0000-0003-2843-134X
ORCID Icon,
Razieh Mohebata Department of Chemistry, Yazd Branch, Islamic Azad University, Yazd, Iran
&
Alireza Hassanabadib Department of Chemistry, Zahedan Branch, Islamic Azad University, Zahedan, IranORCID Iconhttps://orcid.org/0000-0002-8727-2804
ORCID Icon
Pages 442-445 | Received 10 Nov 2022, Accepted 15 Jan 2023, Published online: 30 Jan 2023
 
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Abstract

The reaction between active alkenes such as 2-pyridin-2-yl-methylene-malononitrile or ethyl-2-cyano-3-pyridin-2-yl-acrylate and acetylenic esters in the presence of KSeCN at room temperature provided a simple and efficient one-pot route for the synthesis of highly functionalized selenophenes. The reaction is characterized by mild conditions, short reaction time and tolerance to various functional groups and the products were fully characterized by multinuclear (1H, 13C, and 77Se) NMR spectroscopy.

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