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Journal of Sulfur Chemistry Volume 41, 2020 - Issue 3
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Short Communication

Mixed bases mediated synthesis of thioamides in water

Jiao LiGreen Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou, Henan, People's Republic of ChinaView further author information
,
Xuanhe RenGreen Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou, Henan, People's Republic of ChinaView further author information
,
Ganzhong LiGreen Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou, Henan, People's Republic of ChinaView further author information
,
Helong LiangGreen Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou, Henan, People's Republic of ChinaView further author information
,
Yajie ZhaoGreen Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou, Henan, People's Republic of ChinaView further author information
,
Zhiwu WangGreen Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou, Henan, People's Republic of ChinaCorrespondence[email protected]
View further author information
,
Heng LiGreen Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou, Henan, People's Republic of ChinaCorrespondence[email protected]
View further author information
&
Bingxin YuanGreen Catalysis Center, College of Chemistry, Zhengzhou University, Zhengzhou, Henan, People's Republic of ChinaCorrespondence[email protected]
ORCID Iconhttps://orcid.org/0000-0003-4580-366XView further author information
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Pages 229-237 | Received 10 Dec 2019, Accepted 14 Jan 2020, Published online: 13 Feb 2020
 
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ABSTRACT

A mixed bases mediated protocol is developed to synthesize thioamides from N-aryl or N-alkylamide, aldehyde and elemental sulfur in water. This reaction requires no addition of external oxidant and avoids large excess of amides. Various functional groups and pharmaceutically interesting heteroaromatic rings could be introduced via this efficient procedure.

GRAPHICAL ABSTRACT

Disclosure statement

No potential conflict of interest was reported by the author(s).

Correction Statement

This article has been republished with minor changes. These changes do not impact the academic content of the article.

Additional information

Funding

The authors thank the National Natural Science Foundation of China (No. 21801229) for funding support.

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