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Original Article

Combined structural, electrical, magnetic and optical characterization of bismuth ferrite nanoparticles synthesized by auto-combustion routeFootnote

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Pages 416-421 | Received 16 Jul 2014, Accepted 02 Sep 2014, Published online: 20 Apr 2018

Figures & data

Fig. 1 TG-DTA curves of (a) as-obtained precursor and (b) BFO nanoparticles calcined at 500 °C.

Fig. 2 XRD pattern of BFO nanoparticles calcined at 500 °C; peaks were indexed according to space group R3c (* and #: some traces of secondary phases) and Reitveld refined pattern with refinement parameters (inset).

Fig. 3 TEM micrographs at various magnification scales and SAED pattern of low temperature grown BFO NPs.

Fig. 4 Log(J) versus log(E) curve of BFO nanoparticles at room temperature showing power law dependence, J ∝ En and (inset) symmetric behavior of J versus E plot for both the polarities of applied field.

Fig. 5 (a) Real dielectric constant and loss (tan δ) with log frequencies at room temperature and (b) real dielectric constant as a function of temperature at various frequencies.

Fig. 6 PE loop of BFO nanoparticles measured at room temperature.

Fig. 7 MH hysteresis curve of BFO nanoparticles measured at room temperature.

Fig. 8 UV–vis optical absorbance spectrum and (inset) calculated band gap Eg.

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