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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 36, 2006 - Issue 13
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Original Articles

Silica Sulfate, an Efficient Catalyst for the Trimethylsilylation of Alcohols

Tong‐Shou Jin Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, ChinaCorrespondence[email protected]
,
Ruo‐Fei Tian Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, China
,
Li‐Bin Liu Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, China
,
Ying Zhao Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, China
&
Tong‐Shuang Li Department of Chemistry, College of Chemistry and Environmental Science, Hebei University, Baoding, China
Pages 1823-1828 | Received 23 Oct 2005, Published online: 18 Aug 2006
 
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Abstract

An easy method for the preparation of trimethylsilyl ethers from alcohols and 1,1,1,3,3,3‐hexamethyl‐disilazane (HMDS) using silica sulfate as a catalyst under mild conditions in excellent yields is described.

Acknowledgments

The project was supported by National Natural Science Foundation of China (29872011), Educational Ministry of China, Educational Department of Hebei Province (990104), and Science and Technology Commission of Hebei Province.

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