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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 38, 2008 - Issue 12
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Original Articles

Unexpected Aromatization of 2-Acetoxy-3, 3-dichloro-4-(α-chloroalkyl)tetrahydrofurans to 3-Alkyl-4-chlorofurans with NaI/DMF

Ram N. Ram Department of Chemistry, Indian Institute of Technology, New Delhi, IndiaCorrespondence[email protected]
&
I. Charles Department of Chemistry, Indian Institute of Technology, New Delhi, India
Pages 1946-1951 | Received 31 Jul 2006, Published online: 12 Jun 2008
 
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Abstract

An unexpected aromatization of 2-acetoxy-3,3-dichloro-4-(α-chloroalkyl)tetrahydrofurans to 3-alkyl-4-chlorofurans occurs on heating with sodium iodide in dimethylformamide (DMF) at 120 °C.

ACKNOWLEDGMENT

Financial assistance from the Department of Science and Technology (DST), New Delhi, is gratefully acknowledged.

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