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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 40, 2010 - Issue 11
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Original Articles

Efficient Solid/Liquid Phase-Transfer Catalytic Diazo Transfer Synthesis

Zsuzsa M. Jászay Research Group of Organic Chemical Technology of the Hungarian Academy of Sciences, Budapest, HungaryCorrespondence[email protected]
,
Truong Son Pham Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Katalin Gönczi Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
,
Imre Petneházy Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
&
László Tőke Department of Organic Chemistry and Technology, Budapest University of Technology and Economics, Budapest, Hungary
Pages 1574-1579 | Received 28 Apr 2009, Published online: 06 May 2010
 
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Abstract

A simple and efficient solid/liquid phase-transfer catalytic diazo transfer reaction for the synthesis of diazocarbonyl, diazophosphonyl, and diazophosphinyl compounds is reported.

ACKNOWLEDGMENT

Financial support by the Hungarian Scientific Research Fund (OTKA No. K60284) is gratefully acknowledged.

Notes

a Conversion is based on 1H NMR analysis.

b Conversion is based on 31P NMR analysis.

c New compound.

d With p-acetamidobenzenesulfonyl azide.

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