Advanced search
Publication Cover
Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 41, 2011 - Issue 18
Submit an article Journal homepage
594
Views
8
CrossRef citations to date
0
Altmetric
Original Articles

Amberlyst-15 Catalyzed Cbz Protection of Amines Under Solvent-Free Conditions

Pranja P. BoraDepartment of Chemistry, North Eastern Hill University, Shillong, India
,
Khiangte VanlaldinpuiaDepartment of Chemistry, North Eastern Hill University, Shillong, India
,
Samuel Lalthazuala RokhumDepartment of Chemistry, North Eastern Hill University, Shillong, India
&
Ghanashyam BezDepartment of Chemistry, North Eastern Hill University, Shillong, India
Pages 2674-2683 | Received 26 Apr 2010, Published online: 29 Jun 2011
 
Sample our Physical Sciences journals, sign in here to start your FREE access for 14 days

Abstract

Amberlyst-15 can effectively catalyze Cbz protection of aliphatic and aromatic amines within 10–15 min under solvent-free conditions. The catalyst can be used repeatedly without loss of activity, and the reaction requires no workup and gives excellent yields.

Graphical Abstract

ACKNOWLEDGMENTS

G.B. is grateful to the Council of Scientific and Industrial Research, New Delhi [Scheme No. 0 1 (1992)/05/EMR-II], and the Department of Science and Technology, New Delhi (Scheme No. SR/S1/OC-25/2007), for providing the financial assistance for this work.

Notes

aAll the reactions were conducted at room temperature.

bYield of the purified products.

Log in via your institution

Access through your institution

Log in to Taylor & Francis Online

Restore content access

Restore content access for purchases made as guest
Purchase options * Save for later

PDF download + Online access

  • 48 hours access to article PDF & online version
  • Article PDF can be downloaded
  • Article PDF can be printed
USD 61.00 Add to cart

Issue Purchase

  • 30 days online access to complete issue
  • Article PDFs can be downloaded
  • Article PDFs can be printed
USD 422.00 Add to cart

* Local tax will be added as applicable

Related Research

People also read lists articles that other readers of this article have read.

Recommended articles lists articles that we recommend and is powered by our AI driven recommendation engine.

Cited by lists all citing articles based on Crossref citations.
Articles with the Crossref icon will open in a new tab.