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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 42, 2012 - Issue 13
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Original Articles

Tetrakis(acetonitrile)copper(I) Hexafluorophosphate–Promoted Efficient Synthesis of Amidoalkyl Naphthols Under Solvent-Free Conditions

Ebrahim Soleimani Department of Chemistry, Razi University, Kermanshah, IranCorrespondence[email protected]
&
Mohsen Zainali Department of Chemistry, Razi University, Kermanshah, Iran
Pages 1885-1889 | Received 23 Nov 2010, Published online: 26 Mar 2012
 
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Abstract

An efficient and direct protocol for the preparation of amidoalkyl naphthols employing a multicomponent, one-pot condensation reaction of β-naphthol, aromatic aldehydes, and amides (acetamide, benzamide, and urea) in the presence of tetrakis(acetonitrile)copper(I) hexafluorophosphate [Cu(CH3CN)4PF6] under solvent-free conditions at 80 °C is described. Good yields, short reaction time, and easy workup are advantages of this procedure.

GRAPHICAL ABSTRACT

ACKNOWLEDGMENT

We gratefully acknowledge financial support from the Research Council of Razi University.

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