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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 46, 2016 - Issue 8
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Original Articles

EGB-promoted electrochemical synthesis of 6-thioxo-[1,3,5]-triazinane-2,4 dione derivatives

Najoua SbeiLaboratoire de Chimie Analytique et Electrochimie, Faculté des Sciences de Tunis, Université Tunis El Manar, Campus Universitaire Farhat Hached, Tunis, Tunisia
,
Baya HaouasLaboratoire de Chimie Analytique et Electrochimie, Faculté des Sciences de Tunis, Université Tunis El Manar, Campus Universitaire Farhat Hached, Tunis, Tunisia
,
Khaled BoujlelLaboratoire de Chimie Analytique et Electrochimie, Faculté des Sciences de Tunis, Université Tunis El Manar, Campus Universitaire Farhat Hached, Tunis, Tunisia
,
Belen BataneroDepartment of Organic Chemistry, University of Alcala, Madrid, Spain
&
Mohamed Lamine BenkhoudLaboratoire de Chimie Analytique et Electrochimie, Faculté des Sciences de Tunis, Université Tunis El Manar, Campus Universitaire Farhat Hached, Tunis, TunisiaCorrespondence[email protected]
Pages 673-677 | Received 17 Jan 2016, Published online: 05 May 2016
 
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ABSTRACT

A simple method for the synthesis of 6-thioxo-[1,3,5]-triazinane-2,4-dione derivatives was reported. The electrogenerated cyanomethyl base obtained from electroreduction of neat acetonitrile assisted the reaction between thiourea derivatives and alkyl or aryl isocyanate. This protocol had the advantage of giving good yields using mild conditions. The obtained products have been identified by spectroscopic data, mass spectrometry, and high-resolution mass spectra or elemental analysis.

GRAPHICAL ABSTRACT

Acknowledgment

The authors gratefully acknowledge the Ministry of Higher Education and Scientific Research (MHESR) for the financial support through the Lab No. LR99ES15.

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