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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 46, 2016 - Issue 14
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Original Articles

Copper-catalyzed decarboxylative C−P cross coupling of arylpropiolic acids with dialkyl hydrazinylphosphonates leading to alkynylphosphonates

Weizhu ChenDepartment of Chemistry and Key Laboratory for Chemical Biology of Fujian Province, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen, Fujian, China;Third Institute of Oceanography, State Oceanic Administration, Xiamen, China
,
Dumei MaDepartment of Chemistry and Key Laboratory for Chemical Biology of Fujian Province, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen, Fujian, China
,
Gaobo HuDepartment of Chemistry and Key Laboratory for Chemical Biology of Fujian Province, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen, Fujian, China
,
Zhuan HongThird Institute of Oceanography, State Oceanic Administration, Xiamen, China
,
Yuxing GaoDepartment of Chemistry and Key Laboratory for Chemical Biology of Fujian Province, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen, Fujian, ChinaCorrespondence[email protected]
&
Yufen ZhaoDepartment of Chemistry and Key Laboratory for Chemical Biology of Fujian Province, College of Chemistry and Chemical Engineering, Xiamen University, Xiamen, Fujian, China
Pages 1175-1181 | Received 14 May 2016, Published online: 08 Jul 2016
 
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ABSTRACT

A facile and novel copper-catalyzed decarboxylative coupling of various arylpropiolic acids with readily available dialkyl hydrazinylphosphonates has been developed, providing an attractive synthetic tool for the synthesis of valuable alkynylphosphonates with operational simplicity and mild reaction conditions.

GRAPHICAL ABSTRACT

Acknowledgments

This work was supported by the Chinese National Natural Science Foundation (21202135), the Natural Science Foundation of Fujian Province of China (No. 2013J05031 and No. 2015N0009), and the National Basic Research Program of China (2012CB821600).

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