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High Pressure Research
An International Journal
Volume 39, 2019 - Issue 1
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Articles

Synthesis of NaxMoO3 crystals through high pressure solid-state reaction

, , , , , , & show all
Pages 1-9 | Received 31 May 2018, Accepted 15 Nov 2018, Published online: 29 Nov 2018
 

ABSTRACT

We report growth of high-purity single crystals of the sodium molybdenum bronzes NaxMoO3 through high pressure solid-state reaction routes. Our results demonstrate that the crystallite sizes of NaxMoO3 can rapidly grow to ∼25 μm under a moderate pressure of 4.0 GPa in just 10 min. This discovery provides a starting point for the growth of large single crystals of alkali metal molybdenum bronzes under high pressure.

Disclosure statement

No potential conflict of interest was reported by the authors.

Additional information

Funding

This work was supported by National Natural Science Foundation of China [11602244 and 11702270].

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