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International Journal of Polymer Analysis and Characterization Volume 20, 2015 - Issue 8
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Original Articles

Composites Based on Polystyrene Microspheres with Nano-Scaled Titanium Dioxide

Nataliya S. SerkhachevaDepartment of Macromolecular Compounds, Lomonosov State University of Fine Chemical Technologies, Moscow, Russia
,
Asiya A. GainanovaDepartment of Materials Science and Technology of Functional Materials and Structures, Lomonosov State University of Fine Chemical Technologies, Moscow, Russia
,
Galina M. Kuz’michevaDepartment of Materials Science and Technology of Functional Materials and Structures, Lomonosov State University of Fine Chemical Technologies, Moscow, Russia
,
Vadim V. PodbelskiyDepartment of Software Engineering, National Research University “Higher School of Economics,”Moscow, Russia
,
Nataliya V. SadovskayaDepartment of Materials Science, Karpov Institute of Physical Chemistry, Moscow, Russia
,
Andrey M. ZybinskiyAnalytics Department, N. M. Fedorovsky All-Russian Research Institute of Mineral Raw Materials, Moscow, Russia
,
Elena N. DomoroshchinaDepartment of Materials Science and Technology of Functional Materials and Structures, Lomonosov State University of Fine Chemical Technologies, Moscow, RussiaCorrespondence[email protected]
,
Andrey V. DorokhovDepartment of Inorganic Chemistry, Lomonosov State University of Fine Chemical Technologies, Moscow, Russia
,
Vladimir V. ChernyshevDepartment of General Chemistry, M. V. Lomonosov Moscow State University, Moscow, Russia
,
Nikolay I. ProkopovDepartment of Macromolecular Compounds, Lomonosov State University of Fine Chemical Technologies, Moscow, Russia
&
Aleksandr Yu. Gerval’dDepartment of Macromolecular Compounds, Lomonosov State University of Fine Chemical Technologies, Moscow, Russia
 show all
Pages 743-753 | Received 14 Jul 2015, Accepted 21 Jul 2015, Published online: 30 Oct 2015
 
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Abstract

This study produced for the first time composites based on polystyrene microspheres with nano-sized titania synthesized by sulfate and sol-gel methods, as well as commercial Hombifine N, Hombikat UV100, and Degussa P25. The starting samples and the composites were characterized by X-ray diffraction, scanning electron microscopy, nitrogen adsorption capacity, and IR spectroscopy. The highest content of nano-titanium dioxide both in the bulk and on the surface of microspheres was obtained with the use of Hombikat UV100. This sample has the largest specific surface area and a high content of reactive OH groups. The adsorption properties of composites were investigated.

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