2,749
Views
20
CrossRef citations to date
0
Altmetric
Articles

Oxidative aging of epoxy asphalt

ORCID Icon, , ORCID Icon & ORCID Icon
Pages 1471-1481 | Received 05 Jun 2020, Accepted 02 Aug 2020, Published online: 17 Aug 2020

Figures & data

Table 1. Properties of epoxy binder (type BIX).

Table 2. Name and composition of studied materials.

Figure 1. Schematic illustration of typical asphalt oxidation in-service conditions.

Figure 1. Schematic illustration of typical asphalt oxidation in-service conditions.

Figure 2. IR spectra of (a) asphalt and EA binder, (b) filler and (c) asphalt binder with filler, or asphalt mastic, and EA mastic (after oven-conditioning at 100°C for 480 h).

Figure 2. IR spectra of (a) asphalt and EA binder, (b) filler and (c) asphalt binder with filler, or asphalt mastic, and EA mastic (after oven-conditioning at 100°C for 480 h).

Figure 3. Change of (a) sulfoxide and (b) carbonyl compounds of asphalt (top) and EA binder (bottom) over oven-conditioning at 80°C, 90°C and 100°C.

Figure 3. Change of (a) sulfoxide and (b) carbonyl compounds of asphalt (top) and EA binder (bottom) over oven-conditioning at 80°C, 90°C and 100°C.

Figure 4. Change of (a) sulfoxide and (b) carbonyl compounds of asphalt (top) and EA mastic (bottom) over oven-conditioning at 80°C, 90°C and 100°C.

Figure 4. Change of (a) sulfoxide and (b) carbonyl compounds of asphalt (top) and EA mastic (bottom) over oven-conditioning at 80°C, 90°C and 100°C.

Figure 5. Incremental values of carbonyl compounds asphalt (top) and EA binder (bottom), (a) without and (b) with filler particles, over oven-conditioning at 80°C, 90°C and 100°C.

Figure 5. Incremental values of carbonyl compounds asphalt (top) and EA binder (bottom), (a) without and (b) with filler particles, over oven-conditioning at 80°C, 90°C and 100°C.

Figure 6. –ln(k) versus 1/RT through oven-conditioning for the studied (a) binders and (b) mastics.

Figure 6. –ln(k) versus 1/RT through oven-conditioning for the studied (a) binders and (b) mastics.

Table 3. Kinetic parameters of studied materials.

Figure 7 Master curves of (a) complex modulus and (b) phase angle of studied materials after oven-conditioning for 480 h at 100°C.

Figure 7 Master curves of (a) complex modulus and (b) phase angle of studied materials after oven-conditioning for 480 h at 100°C.

Figure 8. Master curves of (i) complex modulus and (ii) phase angle of (a) EAF20, (b) EAF50, and (c) EAF100 during oven-conditioning for different times.

Figure 8. Master curves of (i) complex modulus and (ii) phase angle of (a) EAF20, (b) EAF50, and (c) EAF100 during oven-conditioning for different times.

Figure 9. Composition dependence of (a) modulus and (b) phase angle at 10 Hz of epoxy asphalt mastics over oven-conditioning at 100°C.

Figure 9. Composition dependence of (a) modulus and (b) phase angle at 10 Hz of epoxy asphalt mastics over oven-conditioning at 100°C.