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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 179, 2004 - Issue 7
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Original Articles

REACTION OF (ORGANYLTHIO)CHLOROACETYLENES WITH ALIPHATIC 1,2-DITHIOLS: A ROUTE TO FUNCTIONALIZED 1,3-DITHIOLANES

Svetlana G. D'yachkova Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russia
,
Nina K. Gusarova Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russia
,
Elena A. Nikitina Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russia
,
Andrei V. Afonin Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russia
,
Eleonora N. Deryagina Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russia
,
Natal'ya V. Russavskaya Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russia
&
Boris A. Trofimov Siberian Branch of the Russian Academy of Sciences, Irkutsk, Russia
 show all
Pages 1355-1360 | Received 01 Nov 2003, Accepted 01 Nov 2003, Published online: 16 Aug 2010
 
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Abstract

(Organylthio)chloroacetylenes react with aliphatic 1,2-dithiols in dimethyl sulfoxide at 20–25°C in the presence of a two-fold molar excess of alkali to form 2-[(alkylthio)methyliden]-1,3-dithiolanes in up to 66% yield.

Financial support from the Ministry of Industry, Science and Technologies of Russian Federation (grants no. NSH-2241.2003.3 and no.MK-1194.2003.03) is gratefully acknowledged.

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