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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 182, 2007 - Issue 3
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Original Articles

A New and Efficient Method for the Protection of Alcohols and Phenols by Using Hexamethyldisilazane in the Presence of Anhydrous Ferric Chloride under Mild Reaction Conditions

Batool Akhlaghinia Department of Chemistry, Damghan University of Basic Sciences, Damghan, Iran
Pages 687-694 | Received 29 Jul 2005, Accepted 21 Aug 2006, Published online: 30 Jan 2007
 
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Abstract

Alcohols and phenols are protected with hexamethyldisilazane in the presence of anhydrous ferric chloride in good to excellent yields in acetonitrile. This method is highly selective for the conversion of primary alcohols in the presence of secondary and tertiary alcohols and also for conversion phenols.

Acknowledgments

The authors gratefully acknowledge the partial support of this study by the Damghan University Research Council.

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