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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 186, 2011 - Issue 2
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Synthesis of New Benzylic Di-, Tri-, and Tetraphosphonic Acids as Potential Chelating Agents

Nabila AliouaneSétif, Faculté des Sciences de l’Ingénieur, Laboratoire d’Électrochimie des Matériaux Moléculaires et des Complexes, Université Ferhat Abbas, Sétif, Algérie
,
Jean-Jacques HélesbeuxUFR Sciences Pharmaceutiques et Ingénierie de la Santé, IFR QUASAV 149, Laboratoire Substances d’Origine Naturelle et Analogues Structuraux, Université d’Angers, Angers, France
,
Tahar DouadiSétif, Faculté des Sciences de l’Ingénieur, Laboratoire d’Électrochimie des Matériaux Moléculaires et des Complexes, Université Ferhat Abbas, Sétif, Algérie
,
Mustayeen A. KhanUFR Sciences Pharmaceutiques et Ingénierie de la Santé, IFR QUASAV 149, Laboratoire Substances d’Origine Naturelle et Analogues Structuraux, Université d’Angers, Angers, France
,
Gilles BouetUFR Sciences Pharmaceutiques et Ingénierie de la Santé, IFR QUASAV 149, Laboratoire Substances d’Origine Naturelle et Analogues Structuraux, Université d’Angers, Angers, France
,
Salah ChafaaSétif, Faculté des Sciences de l’Ingénieur, Laboratoire d’Électrochimie des Matériaux Moléculaires et des Complexes, Université Ferhat Abbas, Sétif, Algérie
&
Olivier DuvalUFR Sciences Pharmaceutiques et Ingénierie de la Santé, IFR QUASAV 149, Laboratoire Substances d’Origine Naturelle et Analogues Structuraux, Université d’Angers, Angers, France
 show all
Pages 354-364 | Received 23 Mar 2010, Accepted 14 Jun 2010, Published online: 19 Feb 2011
 
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Abstract

New di-, tri-, and tetraphosphonic acids were synthesized starting from four o-hydroxymethyl phenol derivatives and obtained in three steps in good overall yield. The phosphonic acids were isolated and purified using semi-preparative C18 HPLC column. The new compounds were characterized using different spectroscopic methods (1H, 13C, and 31P NMR; ESI MS; and MSn, IR).

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