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Original Articles

Microwave-Assisted Synthesis of Some Substituted Sulfamides

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Pages 285-292 | Received 03 Apr 2013, Accepted 24 Jun 2013, Published online: 03 Dec 2013
 

Abstract

Microwave-assisted synthesis of some substituted open-chain and cyclic sulfamides, by amine-exchange reaction, was studied in a modified domestic microwave oven. Reaction times and yields under microwave radiation were compared with classical heating. Synthesis of the sulfamides under microwave irradiation gave better yields with the desired compounds, and in considerably reduced reaction times, than those obtained by classical heating.

[Supplementary materials are available for this article. Go to the publisher's online edition of Phosphorus, Sulfer, and Silicon and the Related Elements for the following free supplemental files: Additional figures.]

GRAPHICAL ABSTRACT

Acknowledgments

We would like to thank the Ondokuz Mayis University (Grant No: F-286) for financial support of this work.

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