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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 192, 2017 - Issue 5
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Original Articles

Polyethylene glycol supported phosphorus chloride: An efficient and recyclable catalyst for the preparation of nitriles from aldoximes

Xiao-Lan ZhangCollege of Chemistry and Chemical Engineering, Shangrao Normal University, Shangrao, P. R. China
,
Shou-Ri ShengCollege of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, P. R. ChinaCorrespondence[email protected]
,
Mei-Hong WeiCollege of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, P. R. China
&
Xiao-Ling LiuCollege of Chemistry and Chemical Engineering, Jiangxi Normal University, Nanchang, P. R. China
Pages 513-517 | Received 26 Aug 2016, Accepted 25 Nov 2016, Published online: 24 Jan 2017
 
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GRAPHICAL ABSTRACT

ABSTRACT

Polyethylene glycol (PEG) supported phosphorus chloride has been developed and used as an efficient and recyclable catalyst for dehydration of various aldoximes into the corresponding nitriles. This protocol has many advantages such as high conversion, high selectivity, short reaction time, mild reaction conditions, and simple experimental procedure.

Funding

Financial support from the National Natural Science Foundation of China (No. 21062007), the Opening Foundation of National Research Center for Carbohydrate Synthesis (No. GJDTZX-KF-201414), the Opening Foundation of Key Laboratory of Functional Small Organic Molecule, Ministry of Education (No. KLFS-KF-201411) and the Research Program of Jiangxi Province Department of Education (No. GJJ11380) is gratefully acknowledged.

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