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Original Articles

Evaluation of TCS/ZnCl2 with Acetic Anhydride as an Acetylating Reagent for Methylene Ketones

, &
Pages 109-116 | Received 01 Jan 2004, Accepted 06 Jun 2004, Published online: 01 Feb 2007
 

Abstract

A new route for the preparation of β -diketones which have applications in organic synthesis by the reaction of methylene ketones, acetic anhydride, TCS and ZnCl 2 in the solvent methylene chloride at room temperature produces the corresponding β -diketones in excellent yield.

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