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Phosphorus, Sulfur, and Silicon and the Related Elements Volume 180, 2005 - Issue 9
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Original Articles

One-Pot Conversion of Aldoximes Into Nitriles via Aldoxime Tosylates Under Microwave Irradiation

Hossein A. Oskooie Department of Chemistry, School of Sciences, Azzahra University, Vanak, Tehran, Iran
,
Majid M. Heravi Department of Chemistry, School of Sciences, Azzahra University, Vanak, Tehran, Iran
,
Zinab Jaddi Department of Chemistry, School of Sciences, Azzahra University, Vanak, Tehran, Iran
&
Mitra Ghassemzadeh Chemistry and Chemical Engineering Research Center of Iran, Tehran, Iran
Pages 1993-1996 | Received 10 Aug 2004, Accepted 16 Sep 2004, Published online: 19 Aug 2006
 
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Silica-gel-supported aldoximes react with tosyl chloride at room temperature to give the corresponding aldoxime tosylates. These supported aldoxime tosylates were directly converted to their corresponding nitriles in high yields under microwave irradiation.

Acknowledgments

We are grateful to partial financial support from the Azzahra University Research Council.

Notes

a Yeilds are based on weight of oximes used.

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