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Scientific Review

New Developments for 2D High-Resolution Neutron Scattering Experiments: Application Case and Experimental Examples from Crystals to Polymer Science

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Pages 17-20 | Published online: 02 Oct 2007
 

Abstract

Neutron detectors designed to observe wide scattering angles are usually mono or linear detectors allowing the study of the reciprocal space along one direction only (linear multidetector or 2 or 3-axis spectrometers). The observation of a scattering plane has been typically developed for small angle neutron scattering experiments (SANS) [Citation1]. The SANS detectors are typically 2-dimensional multidetectors of large dimensions (∼1m × 1m), of relatively large elementary pixel size (∼ 0.01m × 0.01m), and limited pixel number. Because of these large dimensions, the limited number of the pixels, and also of the technique generally employed to select the wavelength (mechanical selectors provide a wavelength dispersion of about Δλ/λ ≈ 10–14%), the SANS resolution is low.

Acknowledgments

We are very grateful to B. Dessus, O. Gal, Marguerite Quilichini, Gerhard Krexner, Arsen Goukasov, Daniel Petitgrand, O. Dial, G. Exil, and G. Pépy for the fruitful discussions and advice.

Notes

1. J. Byrne, Neutrons, Nuclei and Matter: An Exploration of the Physics of Slow Neutrons. Bristol: Institute of Physics Publishing (1993); G.L. Squires, Introduction to the Theory of Thermal Neutron Scattering. Cambridge University Press (1978); J. S. Higgins and H. C. Benoit, Polymers and Neutron Scattering, Clarendon Press - Oxford Science Publications (1994).

3. D. Durand et al., Biopolymers 33, 725–733 (1993); A.M. Micu et al., J. Phys. Chem. 99, 5645 (1995).

4. L. Noirez et al., J. Phys. France 2, 821 (1991); Handbook of Liquid Crystals, eds. D. Demus, J. Goodby, G.W. Gray, H.W. Spiess, and V. Vill. vol. 3, Wiley-Vch.

5. Cambridge Structural Database (5.26 Allen) 2002.

7. “PXY” 2-dimensional data treatment program, G. Pépy, available at the LLB.

8. L. Noirez, Mol. Cryst. Liq. Cryst. 260, 525 (1995); L. Noirez et al., Liq. Cryst. 16, 1081 (1994).

13. V. W. Kuhn and F. Grün, Kolloid. Zeit. 101, 248 (1942); J.P. Ibar, J.M.S.-Rev. Macromol. Chem. Phys. C37, 389 (1997); G. Marrucci and G. Ianniruberto, J. Non-Newtonian Fluid Mech. 82, 275 (1999); H. Mendil et al. Euro. Phys. J. E19, 1 (2006).

14. D.F.R. Mildner and J.M. Carpentier, J. Appl. Cryst. 20, 419 (1987); J. S. Pedersen et al., J. Appl. Cryst. 23, 321 (1990); G. Pépy, J. de Physique, Colloque C5, suppl. n°8, 47, 87–94 (1986).

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