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Integrated Ferroelectrics
An International Journal
Volume 173, 2016 - Issue 1: Proceedings of the International Conference on Functional Materials and Nanotechnologies (FM&NT-2015)
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Original Articles

Nano-indentation studies and macro-scale mechanical testing of calcium modified (Pb0.75Ba0.25)(Zr0.70Ti0.30)O3 ceramics

Z. MachnikInstitute of Technology and Mechatronics, University of Silesia, Sosnowiec, Poland
,
L. KozielskiInstitute of Technology and Mechatronics, University of Silesia, Sosnowiec, Poland
,
M. AdamczykInstitute of Technology and Mechatronics, University of Silesia, Sosnowiec, PolandCorrespondence[email protected]
,
D. BochenekInstitute of Technology and Mechatronics, University of Silesia, Sosnowiec, Poland
,
B. Wodecka-DusInstitute of Technology and Mechatronics, University of Silesia, Sosnowiec, Poland
,
D. RadoszewskaInstitute of Technology and Mechatronics, University of Silesia, Sosnowiec, Poland
,
J. BartkowskaInstitute of Technology and Mechatronics, University of Silesia, Sosnowiec, Poland
&
R. NowakNordic Hysitron Laboratory, Faculty of Chemistry and Materials Science, Helsinki University of Technology, Finland
 show all
Pages 89-95 | Received 05 Oct 2015, Accepted 12 Feb 2016, Published online: 17 Jun 2016
 
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ABSTRACT

The main motivation of present article is to clarify the role of calcium ions in the formation of the mechanical properties of (Pb0.75Ba0.25)(Zr0.70Ti0.30)O3 ceramics. For this purpose the base ceramics as well as ceramics contain 0.5; 1; 2; 3; 4 at.% of calcium were prepared using conventional mixed oxide method. In the experiment, the nanoindentation techniques were applied to evaluate the elastic modulus and hardness values as a function of indentation depth. The results were compared with these in macroscale obtained by ultrasound techniques and shown that not always expensive nanoscale characterisation methods reveal real materials properties in microscale.

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