Publication Cover
Materials Technology
Advanced Performance Materials
Volume 35, 2020 - Issue 11-12
1,226
Views
4
CrossRef citations to date
0
Altmetric
Research Article

Bioactive conformable hydrogel-carbonated hydroxyapatite nanocomposite coatings on Ti-6Al-4V substrates

, , &
Pages 727-733 | Received 14 Mar 2018, Accepted 04 May 2018, Published online: 14 Jun 2018

Figures & data

Figure 1. (a) XRD pattern (solid line) of carbonated hydroxyapatite (CHA) with XRD peaks of synthetic HA (ICDD: 09–0432, dotted line) (b) FTIR spectrum and (c) TEM image of CHA synthesised.

Figure 1. (a) XRD pattern (solid line) of carbonated hydroxyapatite (CHA) with XRD peaks of synthetic HA (ICDD: 09–0432, dotted line) (b) FTIR spectrum and (c) TEM image of CHA synthesised.

Figure 2. PHEMA/PCL-nCHA composite coatings onto Ti-6Al-4V discs (a) 0 wt.% nCHA (b) 5 wt.% nCHA (c) 10 wt.% nCHA; the inset depicting the same composition coating in a tilt view (d) 12 wt.% nCHA (e) 15 wt.% nCHA (f) 20 wt.% nCHA.

Figure 2. PHEMA/PCL-nCHA composite coatings onto Ti-6Al-4V discs (a) 0 wt.% nCHA (b) 5 wt.% nCHA (c) 10 wt.% nCHA; the inset depicting the same composition coating in a tilt view (d) 12 wt.% nCHA (e) 15 wt.% nCHA (f) 20 wt.% nCHA.

Figure 3. AFM images of (a) dry height (b) phase and (c) hydrated height of 0 wt.% nCHA composite coatings (d) dry height and (e) phase of 5 wt.% nCHA composite coatings (f) dry height (g) phase and (h) hydrated height of 10 wt.% nCHA composite coatings.Note: the colour scale on the images is not consistent.

Figure 3. AFM images of (a) dry height (b) phase and (c) hydrated height of 0 wt.% nCHA composite coatings (d) dry height and (e) phase of 5 wt.% nCHA composite coatings (f) dry height (g) phase and (h) hydrated height of 10 wt.% nCHA composite coatings.Note: the colour scale on the images is not consistent.

Figure 4. Load-displacement curves of PHEMA/PCL-nCHA composite coatings in (a) dry and (b) wet conditions, the modulus evaluated for the composite coatings in (c) dry and (d) wet conditions.

Figure 4. Load-displacement curves of PHEMA/PCL-nCHA composite coatings in (a) dry and (b) wet conditions, the modulus evaluated for the composite coatings in (c) dry and (d) wet conditions.

Figure 5. SEM micrographs of primary human osteoblast (HOB) cells on PHEMA/PCL-nCHA composite coating surface with (a) 0 wt.% nCHA (b) 5 wt.% nCHA and (c) 10 wt.% nCHA after 3 days in cell culture, (d) 0 wt.% nCHA (e) 5 wt.% nCHA and (f) 10 wt.% nCHA after 14 days in cell culture.

Figure 5. SEM micrographs of primary human osteoblast (HOB) cells on PHEMA/PCL-nCHA composite coating surface with (a) 0 wt.% nCHA (b) 5 wt.% nCHA and (c) 10 wt.% nCHA after 3 days in cell culture, (d) 0 wt.% nCHA (e) 5 wt.% nCHA and (f) 10 wt.% nCHA after 14 days in cell culture.