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Engineering and Structural materials

Quantitative analysis of {332}〈113〉 twinning in a Ti-15Mo alloy by in situ scanning electron microscopy

ORCID Icon, , , &
Pages 474-483 | Received 16 Feb 2018, Accepted 09 May 2018, Published online: 07 Jun 2018

Figures & data

Figure 1. Scheme of the twin plane trace approach. (a): BSE-SEM image of the twin structure of the SG sample strained to 425 MPa/ε: 0.3%. (b)–(d): Example of twin plane analysis of grain A marked in (a). α exp: angle between surface twin plane trace and rolling direction; α cal: angle between rolling direction and trace projection of the twin plane onto the RD-TD plane; SF: Schmid factor.

Figure 1. Scheme of the twin plane trace approach. (a): BSE-SEM image of the twin structure of the SG sample strained to 425 MPa/ε: 0.3%. (b)–(d): Example of twin plane analysis of grain A marked in (a). α exp: angle between surface twin plane trace and rolling direction; α cal: angle between rolling direction and trace projection of the twin plane onto the RD-TD plane; SF: Schmid factor.

Figure 2. Stress-strain curves of the tensile strained samples.

Notes: The load drops indicate the stress relaxation that occurred when the experiment was paused and BSE-SEM images were taken. SG: Fine-grained sample; LG: Coarse-grained sample.
Figure 2. Stress-strain curves of the tensile strained samples.

Figure 3. ϕ 2 = 45° ODF sections. (a) Annealed SG sample; (b) Annealed LG sample; (c) SG sample, ε: 8.1%; (d) LG sample, ε: 8.8%. (e) Drawing of the most relevant texture orientations in bcc metals located in the ϕ 2 = 45° ODF section.

Figure 3. ϕ 2 = 45° ODF sections. (a) Annealed SG sample; (b) Annealed LG sample; (c) SG sample, ε: 8.1%; (d) LG sample, ε: 8.8%. (e) Drawing of the most relevant texture orientations in bcc metals located in the ϕ 2 = 45° ODF section.

Figure 4. BSE-SEM images of the evolution of {332}〈113〉 twin structure upon deformation in the SG sample. (a) 425 MPa/ε: 0.3%; (b) 495 MPa/ε: 1.4%; (c) 560 MPa/ε: 8.1%. (d) EBSD map along tensile direction. Sample deformed to 495 MPa/ε: 1.4%.

Figure 4. BSE-SEM images of the evolution of {332}〈113〉 twin structure upon deformation in the SG sample. (a) 425 MPa/ε: 0.3%; (b) 495 MPa/ε: 1.4%; (c) 560 MPa/ε: 8.1%. (d) EBSD map along tensile direction. Sample deformed to 495 MPa/ε: 1.4%.

Figure 5. BSE-SEM images of the evolution of {332}〈113〉 twin structure upon deformation in the LG sample. (a) 380 MPa/ε: 0.3%; (b) 430 MPa/ε: 0.9%; (c) 530 MPa/ε: 8.8%. (d) EBSD map along tensile direction. Sample deformed to 530 MPa/ε: 8.8%.

Figure 5. BSE-SEM images of the evolution of {332}〈113〉 twin structure upon deformation in the LG sample. (a) 380 MPa/ε: 0.3%; (b) 430 MPa/ε: 0.9%; (c) 530 MPa/ε: 8.8%. (d) EBSD map along tensile direction. Sample deformed to 530 MPa/ε: 8.8%.

Figure 6. Frequency of the apparent critical resolved shear stress τ c at which primary twins are nucleated and propagated in the SG an LG samples.

Notes: SG: Fine-grained sample; LG: Coarse-grained sample.
Figure 6. Frequency of the apparent critical resolved shear stress τ c at which primary twins are nucleated and propagated in the SG an LG samples.

Figure 7. Twin number fraction as a function of the highest Schmid factor for twinning m(1) of the active twin variants in the SG (a) and LG sample (b), respectively.

Figure 7. Twin number fraction as a function of the highest Schmid factor for twinning m(1) of the active twin variants in the SG (a) and LG sample (b), respectively.

Figure 8. Twin frequency of activated twin variants (v(1) … v(12)) in the SG (a) and LG samples (b), respectively.

Figure 8. Twin frequency of activated twin variants (v(1) … v(12)) in the SG (a) and LG samples (b), respectively.

Figure 9. Evolution of the number of twins n tw with plastic strain, ε, (a) and macroscopic stress, σ, (b).

Notes: SG: Fine-grained sample; LG: Coarse-grained sample.
Figure 9. Evolution of the number of twins n tw with plastic strain, ε, (a) and macroscopic stress, σ, (b).

Figure 10. Evolution of the number of twins per grain boundary area ntwGBwith plastic strain, ε.

Notes: SG: Fine-grained sample; LG: Coarse-grained sample.
Figure 10. Evolution of the number of twins per grain boundary area ntwGBwith plastic strain, ε.