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Fullerenes, Nanotubes and Carbon Nanostructures Volume 15, 2007 - Issue 1
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Original Articles

Isolation and Spectroscopic Characterization of Eu@C72

Karin Bucher Max Planck Institute for Solid State Research, Stuttgart, GermanyCorrespondence[email protected]
,
Jens Mende Physical Institute, University of Stuttgart, Stuttgart, Germany
,
Michael Mehring Physical Institute, University of Stuttgart, Stuttgart, Germany
&
Martin Jansen Max Planck Institute for Solid State Research, Stuttgart, Germany
Pages 29-42 | Received 27 Sep 2005, Accepted 16 Nov 2005, Published online: 12 Jan 2007
 
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Abstract

A new Eu‐endohedral fullerene cage, namely, Eu@C72, was synthesized, separated, and a single isomer, Eu@C72‐I, has been isolated by multi‐step HPLC for the first time and characterized by LDI‐TOF mass spectrometry, UV‐Vis and EPR spectroscopy. Additionally, a second isomer, Eu@C72‐II, has been separated by HPLC and identified by LDI‐TOF mass spectrometry.

Keywords:

Acknowledgments

M.M. would like to acknowledge financial support by the Deutsche Forschungs‐gemeinschaft (DFG) within the High Field EPR Special Project and the Fonds der Deutschen Chemie.

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