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Molecular Crystals and Liquid Crystals Volume 628, 2016 - Issue 1: 13th International Conference on Frontiers of Polymers and Advanced Materials (ICFPAM 2015)
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Original Articles

Pyrene bisiminopyridine ligand and its zinc complex

Awatef AyadiUniversité d'Angers, CNRS UMR 6200, Laboratoire MOLTECH-Anjou, Angers Cedex, France;Laboratoire de Physico-chimie de l'état solide, Université de Sfax, Route de Soukra, Sfax, Tunisia
,
Diana BranzeaUniversité d'Angers, CNRS UMR 6200, Laboratoire MOLTECH-Anjou, Angers Cedex, France
,
Haluk DinçalpDepartment of Chemistry, Faculty of Arts and Science, Celal Bayar University, Muradiye-Manisa, Turkey
,
Nabil ZouariLaboratoire de Physico-chimie de l'état solide, Université de Sfax, Route de Soukra, Sfax, Tunisia
&
Abdelkrim El-GhayouryUniversité d'Angers, CNRS UMR 6200, Laboratoire MOLTECH-Anjou, Angers Cedex, FranceCorrespondence[email protected]
Pages 188-197 | Published online: 13 May 2016
 
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ABSTRACT

The synthesis of a pyrene bisiminopyridine ligand L was successfully accomplished by condensation between 1-aminopyrene and 2,6-pyridinecarboxaldehyde. The complexation of L with zinc triflate afforded a neutral metal complex formulated as [Zn(H2O)LCF3SO3)2].2Et2O. In the complex, the ligand is coordinated to zinc(II) through its three nitrogen atoms which form a distorted octahedral environment together with three oxygen atoms, two from the triflate anions and one from aqua ligand. Both compounds have been characterized using NMR, elemental analysis, mass spectrometry, electronic absorption (UV-Vis) and infrared. Luminescence properties of these compounds show an emission maxima at 412 nm, indicating a pyrene monomer emission.

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