On Wiping the Interior Walls of 37-mm Closed-Face Cassettes: An OSHA Perspective

Abstract

As early as 1976, Occupational Safety and Health Administration (OSHA) methods for analyzing metal samples collected using 37-mm polystyrene closed-face cassettes specified that any loose dust be transferred from the cassette to the digestion vessel, that the cassette be rinsed, and that, if necessary, the cassette be wiped out to help ensure that all particles that enter the cassette are included along with the filter as part of the sample for analysis. OSHA analytical methods for metal analysis were recently revised to explicitly require cassette wiping for all metal samples. This change was based on policy that any material entering the collection device constitutes part of the sample and on OSHA Salt Lake Technical Center research showing that invisible residue on the cassette walls can significantly contribute to the total sample results reported. OSHA procedures are consistent with guidance given in the NIOSH Manual of Analytical Methods. This guidance concludes that internal deposits in sampling cassettes should be included in the analysis and that one way to accomplish this would be to wipe or wash the internal surfaces of the cassette and include the material along with the filter for analysis.

Keywords:

• 37-mm cassette
• cassette rinse
• cassette wipe
• closed-face cassette
• internal cassette walls
• metal analysis

Acknowledgments

This article was presented at the 3rd International Symposium on Beryllium Particulates and Their Detection, November 17–19, 2008, University of New Mexico, Albuquerque, New Mexico.

This article was prepared by U.S. government employees as part of their official duties and legally may not be copyrighted in the United States.