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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 42, 2012 - Issue 1
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Original Articles

Syntheses and Crystal Structures of Two Azide-Bridged Dinuclear Zinc(II) Complexes with Schiff Bases and Halides

Rui-Hua Hui Department of Chemistry, Anshan Normal University, Anshan, P. R. China
,
Peng Zhou Department of Chemistry, Anshan Normal University, Anshan, P. R. China
&
Zhong-Lu You Department of Chemistry and Chemical Engineering, Liaoning Normal University, Dalian, P. R. China
Pages 135-139 | Received 24 Oct 2009, Accepted 28 Jul 2011, Published online: 31 Jan 2012
 
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Abstract

Two end-on azide-bridged dinuclear Schiff base zinc(II) complexes, [Zn2Br2(μ1,1-N3)L1 2]·H2O (1) and [Zn2I2(μ1,1-N3)L2 2]·I (2) (L1 = 4-bromo-2-[(2-isopropylaminoethylimino)methyl]phenol, L2 = 2-ethoxy-6-[(2-ethylaminoethylimino)methyl]phenol), have been synthesized and characterized by elemental analysis, IR spectra, and single-crystal X-ray diffraction. One Zn atom in (1) is five-coordinated in a square pyramidal geometry, while the other Zn atom in (1) and the Zn atoms in (2) are in tetrahedral geometries.

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