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Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry Volume 44, 2014 - Issue 6
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Original Articles

Hydrothermal Synthesis, Crystal Structure, and Luminescence Property of an Mn-Tb Complex Based on 5-(isonicotinamido)-isophthalate

Man-Sheng Chen Department of Chemistry and Materials Science, Hengyang Normal University, Hengyang, China
,
Yi-Fang Deng Department of Chemistry and Materials Science, Hengyang Normal University, Hengyang, China
,
Xue Nie Department of Chemistry and Materials Science, Hengyang Normal University, Hengyang, China
&
Chun-Hua Zhang Department of Chemistry and Materials Science, Hengyang Normal University, Hengyang, China
Pages 868-872 | Received 19 Mar 2013, Accepted 27 Mar 2013, Published online: 25 Feb 2014
 
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Abstract

A 3d-4f heterometallic coordination polymer, [Mn0.5Tb (INAIP)2(H2O)2]·2H2O (1) has been prepared by hydrothermal reactions of the corresponding lanthanide salt with 5-(isonicotinamido)isophthalic acid (H2INAIP) in the presence of MnSO4·H2O and NaOH. X-ray single-crystal structural analysis reveals that 1 features non-interpenetrated three-dimensional (3D) coordination framework containing two-dimensional (2D) (4, 4) Tb-carboxylate layers. In addition, 1 also displayed photoluminescent properties in the green range at room temperature.

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