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Energy Sources, Part A: Recovery, Utilization, and Environmental Effects Volume 34, 2012 - Issue 22
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Original Articles

The Determination of Fatty Acid Methyl Esters in Biodiesel from Rapeseed Oil by Gas Chromatography with a Packed Column

H. Fan College of Chemistry and Chemical Engineering, Nanjing University of Technology, Nanjing, China
,
B. Wang College of Chemistry and Chemical Engineering, Nanjing University of Technology, Nanjing, China
&
Z. Yun College of Chemistry and Chemical Engineering, Nanjing University of Technology, Nanjing, China
Pages 2084-2091 | Received 20 Apr 2010, Accepted 04 Jun 2010, Published online: 24 Sep 2012
 
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Abstract

A method for the determination of fatty acid methyl esters in biodiesel was investigated by gas chromatography using a stainless steel column packed with polydiethylene glycol adipate coated on 102 white support and a flame ionization detector. The linear correlation coefficient was above 0.998, the relative standard deviation was less than 0.46%, and the recovery of standard addition was found to be within 96.8–105.4%. It has good separation efficiency, accuracy, and reproducibility.

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