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Original Articles

A facile approach for the synthesis of uniform hollow β-CuSCN microspheres

, , , &
Pages 789-796 | Received 23 Mar 2011, Accepted 21 Jul 2011, Published online: 28 Jun 2012

Figures & data

Figure 1. A typical XRD profile of the as-prepared β-CuSCN.

Figure 1. A typical XRD profile of the as-prepared β-CuSCN.

Figure 2. (Colour online) (a) Low-magnification SEM image of the sample; (b) high-magnification SEM image of some fragments of hollow spheres; (c) high-magnification SEM image of a typical individual broken sphere; and (d) the microscopic image (×1000).

Figure 2. (Colour online) (a) Low-magnification SEM image of the sample; (b) high-magnification SEM image of some fragments of hollow spheres; (c) high-magnification SEM image of a typical individual broken sphere; and (d) the microscopic image (×1000).

Figure 3. The FT-IR spectrum of the dithizone and the complex: (a) the dithizone and (b) the as-prepared complex.

Figure 3. The FT-IR spectrum of the dithizone and the complex: (a) the dithizone and (b) the as-prepared complex.

Figure 4. SEM images of β-CuSCN hollow spheres prepared at different reaction stages: (a) 5; (b) 8; (c) 11; and (d) 24 h.

Figure 4. SEM images of β-CuSCN hollow spheres prepared at different reaction stages: (a) 5; (b) 8; (c) 11; and (d) 24 h.

Figure 5. Schematic illustration of the possible formation mechanism of CuSCN hollow spheres.

Figure 5. Schematic illustration of the possible formation mechanism of CuSCN hollow spheres.

Figure 6. The UV–vis absorption spectrum of β-CuSCN hollow microstructures.

Figure 6. The UV–vis absorption spectrum of β-CuSCN hollow microstructures.

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