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Original Articles

Synthesis and characterisation of CuS nanomaterials using hydrothermal route

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Pages 329-336 | Received 29 Sep 2011, Accepted 24 Jan 2012, Published online: 02 Jul 2012

Figures & data

Figure 1. XRD of CuS nanostructure synthesised at 150°C for different reaction time (a) 5 h, (b) 16 h and (c) 24 h.

Figure 1. XRD of CuS nanostructure synthesised at 150°C for different reaction time (a) 5 h, (b) 16 h and (c) 24 h.

Figure 2. FE-SEM images of CuS nanostructures synthesised at 150°C for a reaction time of 5 h at different magnifications.

Figure 2. FE-SEM images of CuS nanostructures synthesised at 150°C for a reaction time of 5 h at different magnifications.

Figure 3. FE-SEM images of CuS nanostructures synthesised at 150°C for a reaction time of 16 h at different magnifications.

Figure 3. FE-SEM images of CuS nanostructures synthesised at 150°C for a reaction time of 16 h at different magnifications.

Figure 4. FE-SEM images of CuS nanostructures synthesised at 150°C for a reaction time of 24 h at different magnifications.

Figure 4. FE-SEM images of CuS nanostructures synthesised at 150°C for a reaction time of 24 h at different magnifications.

Figure 5. (Colour online) UV–Vis absorption spectrum of CuS nanomaterial synthesised at 150°C for different reaction time periods.

Figure 5. (Colour online) UV–Vis absorption spectrum of CuS nanomaterial synthesised at 150°C for different reaction time periods.

Figure 6. (Colour online) Cyclic voltammetry (CV curves) of CuS nanostructures synthesised at 150°C for a reaction time of 24 h in 1 M KOH electrolyte.

Figure 6. (Colour online) Cyclic voltammetry (CV curves) of CuS nanostructures synthesised at 150°C for a reaction time of 24 h in 1 M KOH electrolyte.

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