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Original Articles

Effect of reaction conditions on silanisation of sepiolite nanoparticles

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Pages 1171-1183 | Received 13 Jan 2016, Accepted 07 Jun 2016, Published online: 28 Jun 2016

Figures & data

Figure 1. FTIR spectra of pristine sepiolite (PS), modified sepiolite by acidic method (AS) and basic method (BS).

Figure 1. FTIR spectra of pristine sepiolite (PS), modified sepiolite by acidic method (AS) and basic method (BS).

Figure 2. Molecular structure and the corresponding carbonyl FTIR peaks of monomolecular γ-MPS molecules.

Figure 2. Molecular structure and the corresponding carbonyl FTIR peaks of monomolecular γ-MPS molecules.

Figure 3. Thermogravimetric curves of PS, AS and BS.

Figure 3. Thermogravimetric curves of PS, AS and BS.

Figure 4. TGA thermogram of γ-MPS.

Figure 4. TGA thermogram of γ-MPS.

Figure 5. XRD patterns of pristine sepiolite (PS), AS and BS.

Figure 5. XRD patterns of pristine sepiolite (PS), AS and BS.

Figure 6. SEM micrographs of (a) PS, (b) AS and (c) BS.

Figure 6. SEM micrographs of (a) PS, (b) AS and (c) BS.

Figure 7. Separation analyses in LUMI Reader®. Sedimentation behaviour of PS, AS and BS.

Figure 7. Separation analyses in LUMI Reader®. Sedimentation behaviour of PS, AS and BS.

Figure 8. Visual observations of sedimentation of nanosepiolite in ethanol (a) immediately after mixing, (b) after four days, (c) after one week and (d) after one month.

Figure 8. Visual observations of sedimentation of nanosepiolite in ethanol (a) immediately after mixing, (b) after four days, (c) after one week and (d) after one month.

Figure 9. The effect of pH on the zeta potential of modified sepiolite samples.

Figure 9. The effect of pH on the zeta potential of modified sepiolite samples.

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