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Article

Synthesis Of Samarium Oxychloride Nanoplates By Chemical Vapour Deposition

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Pages 33-40 | Received 26 Jan 2019, Accepted 27 Apr 2019, Published online: 24 May 2019

Figures & data

Figure 1. (a) General morphology of deposits, (b) magnified SEM image of the crowded nanoplates.

Figure 1. (a) General morphology of deposits, (b) magnified SEM image of the crowded nanoplates.

Figure 2. (a) Morphology of nanoplates grown at 760 °C for 1 min, (b) TEM image of a single nanoplate, (c) high resolution TEM image, (d) SAED pattern, (e) EDAX spectrum of a nanoplate, (f) AFM image of nanoplates, (right) height plot crossing an edge of a small nanoplate.

Figure 2. (a) Morphology of nanoplates grown at 760 °C for 1 min, (b) TEM image of a single nanoplate, (c) high resolution TEM image, (d) SAED pattern, (e) EDAX spectrum of a nanoplate, (f) AFM image of nanoplates, (right) height plot crossing an edge of a small nanoplate.

Figure 3. SEM image of nanoplates grown on a TEM grid.

Figure 3. SEM image of nanoplates grown on a TEM grid.

Figure 4. (a) Morphology of nanoplates grown with decaborane addition, (b) AFM image of nanoplates, (right) height plot crossing an edge of a nanoplate, (c) and (e) SAED pattern, (d) and (f) high resolution TEM image of the same nanoplate in different zone axis.

Figure 4. (a) Morphology of nanoplates grown with decaborane addition, (b) AFM image of nanoplates, (right) height plot crossing an edge of a nanoplate, (c) and (e) SAED pattern, (d) and (f) high resolution TEM image of the same nanoplate in different zone axis.

Scheme 1. Schematic illustration of SmOCl nanoplate formation. SmOCl Structure: Bi (pink), O (red), Cl (green).

Scheme 1. Schematic illustration of SmOCl nanoplate formation. SmOCl Structure: Bi (pink), O (red), Cl (green).