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Article

Synthesis, characterization, and analysis of zinc oxide nanoparticles using varying pulsed laser ablation energies in liquid

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Article: 2175817 | Received 29 Dec 2022, Accepted 26 Jan 2023, Published online: 17 Oct 2023

Figures & data

Figure 1. Schematic representation of the system setup.

Figure 1. Schematic representation of the system setup.

Figure 2. HR-TEM images of the ZnO NPs produced at (a, d) 70 mJ, (b, e) 90 mJ, and (c, f) 130 mJ. Size distribution of the ZnO NPs obtained using the computer software ‘Image J’, based on several high magnification TEM images at (g) 70 mJ, (h) 90 mJ, and (i) 130 mJ.

Figure 2. HR-TEM images of the ZnO NPs produced at (a, d) 70 mJ, (b, e) 90 mJ, and (c, f) 130 mJ. Size distribution of the ZnO NPs obtained using the computer software ‘Image J’, based on several high magnification TEM images at (g) 70 mJ, (h) 90 mJ, and (i) 130 mJ.

Figure 3. SEM-EDX data of ZnO NPs at (a) 70 mJ, (b) 90 mJ, and (c) 130 mJ.

Figure 3. SEM-EDX data of ZnO NPs at (a) 70 mJ, (b) 90 mJ, and (c) 130 mJ.

Figure 4. HR-TEM images of ZnO NPs (a) at 70 mJ, (b)(c) FFT images of the red square after selecting diffraction spots, (d)(e) the IFFT for selected diffraction spots in b, c, (f) at 90 mJ, (g)(h) FFT images of the blue square after selecting diffraction spots, (i)(j) the IFFT for selected diffraction spots in g, h, (k) at 130 mJ, (l)(m) FFT images of the white square after selecting diffraction spots, (n)(o) the IFFT for selected diffraction spots in (l), (m).

Figure 4. HR-TEM images of ZnO NPs (a) at 70 mJ, (b)(c) FFT images of the red square after selecting diffraction spots, (d)(e) the IFFT for selected diffraction spots in b, c, (f) at 90 mJ, (g)(h) FFT images of the blue square after selecting diffraction spots, (i)(j) the IFFT for selected diffraction spots in g, h, (k) at 130 mJ, (l)(m) FFT images of the white square after selecting diffraction spots, (n)(o) the IFFT for selected diffraction spots in (l), (m).

Figure 5. Zeta-size and zeta-potentials figures of ZnO NPs at different pulsed laser energy.

Figure 5. Zeta-size and zeta-potentials figures of ZnO NPs at different pulsed laser energy.

Figure 6. UV-Visible absorption spectra of the ZnO NPs produced at various laser ablation energies.

Figure 6. UV-Visible absorption spectra of the ZnO NPs produced at various laser ablation energies.

Figure 7. FTIR spectra of the ZnO NPs at various laser ablation energies.

Figure 7. FTIR spectra of the ZnO NPs at various laser ablation energies.

Availability of data and materials

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