Figures & data
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Figure 1. (a) The low-magnification IPF map of HL-Mg-alloy; (b) The grain-size distribution in FG and CG layers. (c) The (0002) PFs of the FG and CG layers, respectively. (d) and (e) The IPF maps of as-rolled sample and as-annealed sample. (f) and (g) The high-magnification IPF and corresponding SEM microstructure of typical region. (h) and (i) TEM analysis showing Mg17Al12 particles mainly distributed along GBs of FGs.
![Figure 1. (a) The low-magnification IPF map of HL-Mg-alloy; (b) The grain-size distribution in FG and CG layers. (c) The (0002) PFs of the FG and CG layers, respectively. (d) and (e) The IPF maps of as-rolled sample and as-annealed sample. (f) and (g) The high-magnification IPF and corresponding SEM microstructure of typical region. (h) and (i) TEM analysis showing Mg17Al12 particles mainly distributed along GBs of FGs.](/cms/asset/9cce9ae4-4272-41e7-a4af-9c387ce34500/tmrl_a_2133976_f0001_oc.jpg)
Figure 2. (a) Engineering stress–strain (σ–ϵ) curves of CG, FG and HL samples and LUR σ–ϵ curve of HL sample under tension along RD; the inset of a shows HDI-stress and HDI/strain-hardening curves of HL sample. (b) Comparison of yield strengths and fracture elongations of the present HL-Mg-alloy (indicated by star) with representative AZ91 Mg-alloys processed by accumulative rolling bonding (ARB) [Citation24,Citation25], equal channel angular process (ECAP) [Citation26–28], extrusion [Citation29–31], high-ratio differential speed rolling (HRDSR) [Citation6,Citation7], and wrought AZ80 [Citation4,Citation5,Citation32], AZ31 [Citation33–36], gradient-structured [Citation10–12] and bimodal-structured Mg-Al-Zn alloys [Citation19–21] reported in literature.
![Figure 2. (a) Engineering stress–strain (σ–ϵ) curves of CG, FG and HL samples and LUR σ–ϵ curve of HL sample under tension along RD; the inset of a shows HDI-stress and HDI/strain-hardening curves of HL sample. (b) Comparison of yield strengths and fracture elongations of the present HL-Mg-alloy (indicated by star) with representative AZ91 Mg-alloys processed by accumulative rolling bonding (ARB) [Citation24,Citation25], equal channel angular process (ECAP) [Citation26–28], extrusion [Citation29–31], high-ratio differential speed rolling (HRDSR) [Citation6,Citation7], and wrought AZ80 [Citation4,Citation5,Citation32], AZ31 [Citation33–36], gradient-structured [Citation10–12] and bimodal-structured Mg-Al-Zn alloys [Citation19–21] reported in literature.](/cms/asset/e431caa5-bebb-4168-99cd-6e1624e7a2d5/tmrl_a_2133976_f0002_oc.jpg)
Figure 3. (a) The IPF map, (b) scalar disclination density (in rad μm−2) and (c) scalar GND density (in μm−1) of the undeformed HL-Mg-alloy; (d) The IPF map, (e) scalar disclination density (in rad μm−2) and (f) scalar GND density (in μm−1) of the ∼3.5% strained HL-Mg-alloy.
![Figure 3. (a) The IPF map, (b) scalar disclination density (in rad μm−2) and (c) scalar GND density (in μm−1) of the undeformed HL-Mg-alloy; (d) The IPF map, (e) scalar disclination density (in rad μm−2) and (f) scalar GND density (in μm−1) of the ∼3.5% strained HL-Mg-alloy.](/cms/asset/55fb9e4f-bd5f-4b8e-b454-96de71d49c95/tmrl_a_2133976_f0003_oc.jpg)
Figure 4. (a) The dark-field TEM image of typical FG after ∼13% tensile deformation under the two-beam condition of g = [].(b) The bright-field TEM image of region (b) in (a) using g = [
]; (c) the dark-field TEM image of region (c) in (a) using g = [
]. (d) The dark-field TEM image of typical FG after ∼23% tensile deformation using g = [
].
![Figure 4. (a) The dark-field TEM image of typical FG after ∼13% tensile deformation under the two-beam condition of g = [101¯0].(b) The bright-field TEM image of region (b) in (a) using g = [0002]; (c) the dark-field TEM image of region (c) in (a) using g = [0002]. (d) The dark-field TEM image of typical FG after ∼23% tensile deformation using g = [0002].](/cms/asset/929d66a3-ef41-4ff1-ae60-d739b780f995/tmrl_a_2133976_f0004_oc.jpg)
Figure 5. (a) The statistical results of the identified slip activity in CG and FG layers. Relative frequencies of activated pyramidal <c+a> slips with high m values (>0.2, above the blue line) and low m values (<0.2, below the blue line) are marked in (a). (b) The slip transfers in a typical region of CG layer. (c)–(f) The IPF, scalar disclination density (in rad µm−2), scalar GND density (in µm−1) and SEM of representative CG near hetero-interface, with feather-shaped tension twinning activated. The white numbers represent values (Schmid factor) under uniaxial loading.
![Figure 5. (a) The statistical results of the identified slip activity in CG and FG layers. Relative frequencies of activated pyramidal <c+a> slips with high m values (>0.2, above the blue line) and low m values (<0.2, below the blue line) are marked in (a). (b) The slip transfers in a typical region of CG layer. (c)–(f) The IPF, scalar disclination density (in rad µm−2), scalar GND density (in µm−1) and SEM of representative CG near hetero-interface, with feather-shaped tension twinning activated. The white numbers represent m values (Schmid factor) under uniaxial loading.](/cms/asset/a26b9ebd-9eda-4dae-a78e-55ecf357a7ca/tmrl_a_2133976_f0005_oc.jpg)