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Full Length Articles

Heterocoagulation and SPS sintering of sulfonitric-treated CNT and 8YZ nanopowders

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Pages 238-246 | Received 17 Dec 2018, Accepted 19 Mar 2019, Published online: 21 Apr 2019

Figures & data

Figure 1. Scheme of the electrostatic heterocoagulation method used to disperse the individual CNTs uniformly within the ceramic powder: aqueous suspensions of treated CNT and 8YZ powder; and mixture of the two suspensions during stirring and after 30 min of stirring, when the composite powder heterocoagulated.

Figure 1. Scheme of the electrostatic heterocoagulation method used to disperse the individual CNTs uniformly within the ceramic powder: aqueous suspensions of treated CNT and 8YZ powder; and mixture of the two suspensions during stirring and after 30 min of stirring, when the composite powder heterocoagulated.

Figure 2. Palmqvist crack at Vickers indentation.

Figure 2. Palmqvist crack at Vickers indentation.

Figure 3. Zeta potentials of treated CNTs (at three temperatures: 50, 90 and 130°C) and 8YZ suspensions at various pH values. The dotted outline zone corresponds to the possible working pH range (pH ~ 4.5).

Figure 3. Zeta potentials of treated CNTs (at three temperatures: 50, 90 and 130°C) and 8YZ suspensions at various pH values. The dotted outline zone corresponds to the possible working pH range (pH ~ 4.5).

Figure 4. TEM images of 8YZ-CNT130 heterocoagulated powder at different magnifications.

Figure 4. TEM images of 8YZ-CNT130 heterocoagulated powder at different magnifications.

Figure 5. SEM micrographs of the fracture surfaces of SPS-consolidated composites at low and high magnifications: a-b) 8YZ-CNT50, c-d) 8YZ-CNT90 and e-f) 8YZ-CNT130.

Figure 5. SEM micrographs of the fracture surfaces of SPS-consolidated composites at low and high magnifications: a-b) 8YZ-CNT50, c-d) 8YZ-CNT90 and e-f) 8YZ-CNT130.

Figure 6. Vickers hardnesses (Hv) of 8YZ and 8YZ-CNT50, 8YZ-CNT90, 8YZ-CNT130 composites.

Figure 6. Vickers hardnesses (Hv) of 8YZ and 8YZ-CNT50, 8YZ-CNT90, 8YZ-CNT130 composites.

Figure 7. Flexural strength of 8YZ and 8YZ-CNT50, 8YZ-CNT90 and 8YZ-CNT130 composites.

Figure 7. Flexural strength of 8YZ and 8YZ-CNT50, 8YZ-CNT90 and 8YZ-CNT130 composites.

Figure 8. Fracture toughness (KIc) of 8YZ and 8YZ-CNT90 and 8YZ-CNT130 composites.

Figure 8. Fracture toughness (KIc) of 8YZ and 8YZ-CNT90 and 8YZ-CNT130 composites.