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Inorganic and Nano-Metal Chemistry Volume 50, 2020 - Issue 3
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Short Communication

Synthesis, crystal structure and theoretical calculation of triphenyltin (IV) polymer based on 2,4-dichlorophenylacrylic acid

Shuang Hana Department of Chemistry, Jilin Normal University, Siping, PR China; ;b Key Laboratory of Preparation and Application of Environmental Friendly Materials, Ministry of Education, Jilin Normal University, Changchun, China
,
He Wanga Department of Chemistry, Jilin Normal University, Siping, PR China; ;b Key Laboratory of Preparation and Application of Environmental Friendly Materials, Ministry of Education, Jilin Normal University, Changchun, China
,
Jiajun Wanga Department of Chemistry, Jilin Normal University, Siping, PR China; ;b Key Laboratory of Preparation and Application of Environmental Friendly Materials, Ministry of Education, Jilin Normal University, Changchun, China
,
Linan Duna Department of Chemistry, Jilin Normal University, Siping, PR China; ;b Key Laboratory of Preparation and Application of Environmental Friendly Materials, Ministry of Education, Jilin Normal University, Changchun, China
,
Chuanbi Lia Department of Chemistry, Jilin Normal University, Siping, PR China; ;b Key Laboratory of Preparation and Application of Environmental Friendly Materials, Ministry of Education, Jilin Normal University, Changchun, China
&
Chunling Liua Department of Chemistry, Jilin Normal University, Siping, PR China; ;b Key Laboratory of Preparation and Application of Environmental Friendly Materials, Ministry of Education, Jilin Normal University, Changchun, ChinaCorrespondence[email protected]
Pages 187-193 | Received 29 Oct 2019, Accepted 09 Dec 2019, Published online: 23 Dec 2019
 
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Abstract

Reaction between 2,4-dichlorophenylacrylic acid (HL) and triphenyltin (IV) hydroxide to yield the complex [(Ph3Sn)L]n (1). The complex has been characterized by elemental analysis, infrared spectrum and single crystal X-ray diffraction. The structural analysis shows that complex 1 possesses 1 D chain structure in which every tin atom is five coordinated. The 1 D chains linked by C(66)-H(66)·Cl(2) hydrogen bonds to aggregate in 2 D framework. Additionally, the PXRD, TG, and luminescent property were also investigated. The quantum chemistry calculations was performed with the Gaussian09 program.

Acknowledgments

We thank the National Natural Science Foundation of China (No. 21805110) for financial support.

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