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Research Article

Mechanical properties of sinter hardened sintered steels prepared by hybrid alloying

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Article: 2202714 | Received 01 Nov 2022, Accepted 08 Apr 2023, Published online: 15 May 2023

Figures & data

Table 1. Chemical composition of the masteralloy used (wt %).

Table 2. Composition of the mixtures used in study 1.

Table 3. Designation and composition of the mixtures used in study 2.

Figure 1. Final geometry (machined and polished) of the fatigue samples for Astaloy CrA + 0.6%C + 3%Ni sinter hardened at 1250 °C.

Figure 1. Final geometry (machined and polished) of the fatigue samples for Astaloy CrA + 0.6%C + 3%Ni sinter hardened at 1250 °C.

Figure 2. Equipment for ultrasonic fatigue testing.

Figure 2. Equipment for ultrasonic fatigue testing.

Figure 3. Hardness, impact energy and oxygen content of PM steels with 0.6% admixed carbon, compacted at 700 MPa, sintered 60 min at 1250 °C in N2-10% H2.

Figure 3. Hardness, impact energy and oxygen content of PM steels with 0.6% admixed carbon, compacted at 700 MPa, sintered 60 min at 1250 °C in N2-10% H2.

Table 4. As-sintered properties of PM steels AstaloyCrA-x-0.6%C (x = Ni, Mn, MA in varying contents). Compacted at 700 MPa, sintered 1 hr at 1250 °C in N2-10%H2.

Figure 5. Impact fracture surfaces of PM steels with 0.6% admixed carbon, compacted at 700 MPa, sintered 60 min at 1250 °C in N2-10% H2.

Figure 5. Impact fracture surfaces of PM steels with 0.6% admixed carbon, compacted at 700 MPa, sintered 60 min at 1250 °C in N2-10% H2.

Figure 6. As-polished OM micrographs of hybrid alloyed steels; the larger pores in Mn steel compared to the two other grades are clearly visible.

Figure 6. As-polished OM micrographs of hybrid alloyed steels; the larger pores in Mn steel compared to the two other grades are clearly visible.

Table 5. Sintered properties of hybrid alloyed steels; compacted at 700 MPa, sintered 60 min at 1250 °C in N2-10%H2, heat treated by gas quenching and tempering

Figure 7. Nital etched OM micrographs of different steels show martensitic matrix after sinter hardening.

Figure 7. Nital etched OM micrographs of different steels show martensitic matrix after sinter hardening.

Figure 8. Soft Ni-rich austenitic area in the microstructure of CrA-3Ni-0.6C.

Figure 8. Soft Ni-rich austenitic area in the microstructure of CrA-3Ni-0.6C.

Figure 9. Impact fracture surfaces of different steels, sinter hardened (broken at RT).

Figure 9. Impact fracture surfaces of different steels, sinter hardened (broken at RT).

Figure 10. S/N curves of different steels, compacted at 700 MPa, sintered 60 min in N2-10% H2 at 1250 °C, gas quenched and tempered.

Figure 10. S/N curves of different steels, compacted at 700 MPa, sintered 60 min in N2-10% H2 at 1250 °C, gas quenched and tempered.

Figure 11. Fatigue fracture surfaces of hybrid alloyed sintered steels, compacted at 700 MPa, sintered 60 min in N2-10% H2 at 1250 °C, gas quenched and tempered.

Figure 11. Fatigue fracture surfaces of hybrid alloyed sintered steels, compacted at 700 MPa, sintered 60 min in N2-10% H2 at 1250 °C, gas quenched and tempered.